| 舒筋壮骨丸质量标准研究 |
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| 引用本文： | 彭腾,张旭,邓赟.舒筋壮骨丸质量标准研究[J].中国药房,2008,19(24):1882-1884. |
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| 作者姓名： | 彭腾 张旭 邓赟 |
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| 作者单位： | 成都中医药大学药学院,成都市,610075 |
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| 摘 要： | 目的:建立舒筋壮骨丸的质量标准。方法:采用薄层色谱(TLC)法对舒筋壮骨丸中的补骨脂、三七、当归、香附、续断进行定性鉴别,以高效液相色谱(HPLC)法对其主药补骨脂中的补骨脂素进行含量测定。结果:定性鉴别分离度好,专属性强;补骨脂素进样量在0.04~0.28μg范围内与峰面积积分值呈良好的线性关系(r=0.9992);平均回收率为98.84,RSD=2.17%。结论:所建标准可用于舒筋壮骨丸的质量控制。
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| 关 键 词： | 舒筋壮骨丸 薄层色谱法 高效液相色谱法 补骨脂素 质量标准 |
Quality Standard of Shujin Zhuanggu Pill |
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| PENG Teng,ZHANG Xu,DENG Yun.Quality Standard of Shujin Zhuanggu Pill[J].China Pharmacy,2008,19(24):1882-1884. |
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| Authors: | PENG Teng ZHANG Xu DENG Yun |
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| Institution: | (School of Pharmacy, Chengdu University of TCM, Chengdu 610075, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Shujinzhuanggu pill. METHODS： Thin- layer chromatography（TLC） was employed for the qualitative determination of Psoralea corylifolia, Panax notoginseng, Angelica sinensis, Cyperus rotundus and Dipsacus asperoides. High performance liquid chromatography（HPLC） was applied for the determination of Psoralen in psoralea corylifolia in Shujin zhuanggu pill. RESULTS： The characteristic identification by TLC was distinctive and highly specific. The linear range of Psoralen was 0.04--0.28μg （r=0.999 2） . The average recovery was 98.84 and RSD was 2.17%. CONCLUSION ：The established standard can be used for the quality control of Shujin zhuanggu pill. |
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| Keywords: | Shujin zhuanggu pill TLC HPLC Psoralen Quality standards |
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