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| GC法测定丁蔻理中丸中丁香酚的含量 | |
| 引用本文： | 林生文,李逸,朱炳辉,李玮玲.GC法测定丁蔻理中丸中丁香酚的含量[J].中国药品标准,2003,4(5):38-40. |
| 作者姓名： | 林生文 李逸 朱炳辉 李玮玲 |
| 作者单位： | 1. 广东省药品检验所,广州,510180 2. 中山大学,广州,510275 3. 中国药科大学,南京,210038 |
| 摘 要： | 目的：采用气相色谱法测定丁蔻理中丸中丁香酚的含量。方法：气相色谱法，聚乙二醇(PEG)—20M柱，柱长2m，内径4mm；柱温180℃，进样器220℃，FID检测器；柱头压力：150kPa，内标物：桂皮醛。结果：所测丁香酚与其它组分具有良好的分离效果，线性范围为8.92～71．36μg／ml，平均回收率为99．9％，RSD为1．28％(n=5)。结论：本方法简便、快速，结果准确，可用于丁蔻理中丸中丁香酚的含量测定。 |
| 关 键 词： | 丁蔻理中丸 中药制剂 丁香酚 含量测定 气相色谱法 |
Determination of Eugenol in Dingkou Lizhong Wan by GC |
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| Authors: | Lin ShengWen Li Yi Zhu Binghui and Li Weiling |
| Institution: | Guangdong Institute for Drug Control, Guangzhou 510180;Zhongshan university, guangzhou 510275;Guangdong Institute for Drug Control, Guangzhou 510180;China Pharmaceutical university, Nanjing 210038 |
| Abstract: | Objective: The purpose is to develop GC method for the assay of eugenol in Dingkou Lizhong Wan.Method: GC was applied to quantitative analysis.Chromatographic conditions were:PEG-20M(2m×4mm);column temperature;180℃;Injector temperature;220℃;Flame ionization detector(FID);Nitrogen was used as carrier gas,the pressure of coloum was 150kPa.The internal standard was cinnamaldehyde.Results: The calibration curve of eugenol had a good linear relationship,and it was well separated from other constituents.The average recovery is 99.9% with RSD=1.28%(n=5).Conclusion: The established method is accuracy and it can be applied to the content determination of eugenol in Dingkou Lizhong Wan. |
| Keywords: | Dingkou Lizhong Wan eugenol GC Determination of content |
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