| HPLC测定小建中胶囊中芍药苷的含量 |
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| 引用本文： | 赵仙文.HPLC测定小建中胶囊中芍药苷的含量[J].山西中医学院学报,2011,12(6):18-19. |
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| 作者姓名： | 赵仙文 |
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| 作者单位： | 山西省朔州市朔城区北城医院,山西 朔州,030062 |
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| 摘 要： | 目的:建立以高效液相色谱法测定小建中胶囊中芍药苷含量的方法。方法:色谱柱为Kromasil C18,流动相为乙腈-0.1%磷酸溶液,检测波长为260 nm。结果:芍药苷在0.1μg/mL~1.2μg/mL范围内线性关系良好(r=0.999 5),平均加样回收率为99.895%,RSD为0.9%(n=6)。结论:本方法简便、灵敏、准确,可用于小建中胶囊的质量控制。
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| 关 键 词： | 高效液相色谱法 小建中胶囊 芍药苷 |
Determination of Paeoniflorin Content in Xiaojianzhong Capsule by HPLC |
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| Zhao Xianwen.Determination of Paeoniflorin Content in Xiaojianzhong Capsule by HPLC[J].Journal of Shanxi College of Traditional Chinese Medicine,2011,12(6):18-19. |
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| Authors: | Zhao Xianwen |
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| Institution: | Zhao Xianwen(Hospital of North Region Office,Shuo Urban District,Shuozhou Shanxi 030062) |
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| Abstract: | Objective：To establish a method for determination of paeoniflorin content in Xiaojianzhong capsule.Method：HPLC was performed on Kromasil C18 column with acetonitrile-0.1% phosphoric acid as mobile phase,detection wavelength was set at 260 nm.Result：The linear range of paeoniflorin was 0.1 μg/mL~1.2 μg/mL（r=0.999 5）,average recovery rate was 99.895%,RSD was 0.9%（n=6）.Conclusion：This method is simple,sensitive,accurate,and can be used for quality control of Xiaojianzhong capsule. |
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| Keywords: | HPLC Xiaojianzhong capsule paeoniflorin |
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