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| 杏叶防风挥发油成分SPME-GC-MS分析 | |
| 引用本文： | 赵超,陈华国,程力,周欣,杨再波,张怡莎.杏叶防风挥发油成分SPME-GC-MS分析[J].中国中药杂志,2007,32(17):1759-1762. |
| 作者姓名： | 赵超 陈华国 程力 周欣 杨再波 张怡莎 |
| 作者单位： | 1. 贵州师范大学,天然药物质量控制研究中心,贵州,贵阳,550001 2. 贵阳中医学院,第二附属医院,贵州,贵阳,550002 3. 黔南民族师范学院,化学与化工系,贵州,都匀,558000 |
| 摘 要： | 目的：分析杏叶防风挥发油化学成分。方法：利用固相微萃取-气相色谱-质谱(SPME-GC-MS)联用技术对杏叶防风挥发油成分进行研究。结果：共鉴定出65种化学成分,占挥发油总成分的92.17%。结论：杏叶防风挥发油主要化学成分是α-姜烯(24.82%),前盖介烯(16.27%),β-没药烯(4.82%),2-异丙基-5-甲基-9-亚甲基-二环［4.4.0］萘烷-1-烯(4.03%),β-倍半水芹烯(3.98%),反式-β-金合欢烯(3.68%),芳姜黄烯(3.54%)等。 |
| 关 键 词： | 杏叶防风 挥发油 固相微萃取 气相色谱-质谱联用 |
| 文章编号： | 1001-5302（2007）17-1759-04 |
| 收稿时间： | 2007-03-12 |
| 修稿时间： | 2007年3月12日 |
Analysis of volatile oil in herb of Pimpinella candolleana by SPME-GC-MS |
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| ZHAO Chao; CHEN Hua-guo; CHENG Li; ZHOU Xin; YANG Zai-bo; ZHANG Yi-sha.Analysis of volatile oil in herb of Pimpinella candolleana by SPME-GC-MS[J].China Journal of Chinese Materia Medica,2007,32(17):1759-1762. | |
| Authors: | ZHAO Chao; CHEN Hua-guo; CHENG Li; ZHOU Xin; YANG Zai-bo; ZHANG Yi-sha |
| Institution: | 1. Research Center of the Quality Control of Natural Medicines, Guizhou Normal University, Guiyang 550001, China; 2. The Second Affiliated Hospital, Guiyang Traditional Medical College, Guiyang 550002, China; 3. Chemistry and Chemical Engineering Department, Qianuan Normal Univesity for Nationalities, Duyun 558000, China |
| Abstract: | OBJECTIVE: To analyze components of volatile oil from the herb of Pimpinella candolleana. Method: The components of volatile oil were investigated by SPME-GC-MS. RESULT: Sixty-five compounds were identified which accounted for 92. 17% of total volatile oil. CONCLUSION: The main constituents in the essential oil were alpha-zingiberene (24.82%), pregeijerene (16.27%), beta-bisabolene (4. 82%), 2-isopropyl-5-methyl-9-methylene-bicyclo 4. 4. 0] dec-l-ene (4.03%), beta-sesquiphellandrene (3.98%), trans-beta-farnesene (3.68%), ar-curcumene (3.54%). |
| Keywords: | Pimpinella candolleana volatile oil SPME GC-MS |
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