| 祛痹颗粒质量标准的研究 |
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| 引用本文： | 肖振良,武卫,周海蓉,刘江. 祛痹颗粒质量标准的研究[J]. 齐鲁药事, 2005, 24(9): 537-539 |
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| 作者姓名： | 肖振良 武卫 周海蓉 刘江 |
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| 作者单位： | 1. 山东中医药大学附属医院,济南,250011
2. 山东省千佛山医院,济南,250014 |
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| 摘 要： | 目的建立控制祛痹颗粒的质量标准。方法采用薄层色谱法对制剂中白芍、丹参进行了定性鉴别,应用高效液相色谱法对金银花中的绿原酸进行了定量测定。结果绿原酸在0.0418~0.209μg范围内线性关系良好,平均回收率达98.3%,RSD=1.71%。结论所建立的方法可行、重复性好,能有效地控制该制剂的质量。
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| 关 键 词： | 祛痹颗粒 芍药苷 原儿茶醛 绿原酸 高效液相色谱法 |
| 文章编号： | 1672-7738(2005)09-0537-03 |
Study on quality standard for Qubi Granules |
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| Xiao Zhen-liang,Wu Wei,Zhou Hai-rong,Liu Jiang. Study on quality standard for Qubi Granules[J]. qilu pharmaceutical affairs, 2005, 24(9): 537-539 |
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| Authors: | Xiao Zhen-liang Wu Wei Zhou Hai-rong Liu Jiang |
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| Affiliation: | 1.The Affiliated Hospital of Shandong University of Traditional Chinese Medicine,Ji' nan,250011;2.Shandong Provincial QianFoshan Hospital,Ji'nan,250011 |
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| Abstract: | Objective To establish the standard for quality control of Qubi Granules.Methods Paeonide Alba and Salvia miltiorrhiza Bge.in the preparation were identified by TLC.The Chlorogenic acid in the Flos Lonicerae was determined by HPLC.Results A good linear range was shown at the concentration from 0.0418μg to 0.209μg.The average recovery was 98.3% and the RSD was 1.71%.Conclusion The methods are available,have good reproducibilities and can be used to control the quality of this granule effectively. |
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| Keywords: | Qubi Granules Peaoniflorin Protocatechuic aldehyde Chlorogenic acid HPLC |
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