| 川丹灵胶囊的质量标准研究 |
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| 引用本文： | 苏华,侯中华,陈翠,王曙东.川丹灵胶囊的质量标准研究[J].中国药房,2012(35):3348-3349. |
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| 作者姓名： | 苏华 侯中华 陈翠 王曙东 |
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| 作者单位： | 南京军区南京总医院制剂科,南京210002 |
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| 摘 要： | 目的:建立川丹灵胶囊的质量标准。方法:采用薄层色谱(TLC)法对方中丹参进行定性鉴别;采用高效液相色谱法测定制剂中腺苷的含量。结果:TLC斑点清晰、分离度好,阴性对照无干扰;腺苷检测浓度在20.42～102.10μg·mL-1范围内与峰面积积分值呈良好的线性关系(r=0.9999),平均加样回收率为101.8%,RSD=2.05%(n=9)。结论:所建标准可用于川丹灵胶囊的质量控制。
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| 关 键 词： | 川丹灵胶囊 薄层色谱法 腺苷 高效液相色谱法 |
Study on Quality Standard of Chuandanling Capsules |
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| SU Hua,HOU Zhong-hua,CHEN Cui,WANG Shu-dong.Study on Quality Standard of Chuandanling Capsules[J].China Pharmacy,2012(35):3348-3349. |
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| Authors: | SU Hua HOU Zhong-hua CHEN Cui WANG Shu-dong |
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| Institution: | (Dept. of Pharmaceutical Preparation, Nanjing Gener- al Hospital of Nanjing Military Command, Nanjing 210002, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Chuandanling capsules. METHODS： Qualitative identification of Salvia miltiorrhiza was conducted by TLC. The content of adenosine was determined by HPLC. RESULTS： The developed TLC spots were clear, well-separated and free from interference of negative sample. The linear range of adenosine was 20.42-102.10 μg.mL^-1（r=0.999 9） with an average recovery of 101.8% （RSD=2.05% ,n=9）. CONCLUSION： The established standard can be used for quality control of Chuandanling capsules. |
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| Keywords: | Chuandanling capsules TLC Adenosine HPLC |
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