| 东北山梅花根化学成分的研究 |
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| 引用本文： | 张庆镐,韩荣弼,刘冬梅,吴学.东北山梅花根化学成分的研究[J].辽宁中医杂志,2007,34(11):1616-1617. |
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| 作者姓名： | 张庆镐 韩荣弼 刘冬梅 吴学 |
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| 作者单位： | 延边大学,吉林,延吉,133002 |
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| 摘 要： | 目的:研究东北山梅花(Philadelphus schrenkii Rupr.)根的化学成分。方法:利用水蒸气蒸馏法提取挥发油,乙醚萃取,所得部分通过GC-MS分析检测;利用硅胶柱色谱结合制备薄层层析分离非挥发性化学成分,光谱分析鉴定结构。结果得到8个挥发油成分,2个非挥发性化合物,分别为香兰素和7-羟基-8-甲氧基香豆素。结论:以上所得挥发油成分和化合物均为首次从东北山梅花根中分离鉴定。
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| 关 键 词： | 东北山梅花 香兰素 7-羟基-8-甲氧基香豆素 挥发油 |
| 文章编号： | 1000-1719（2007）11-1616-02 |
| 修稿时间： | 2007-06-15 |
Studies on the Chemical Constituents of Philadelphus Schrenkii Rupr. Root |
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| ZHANG Qing-gao,HAN Rong-bi,Liu Dong-mei,WU Xue.Studies on the Chemical Constituents of Philadelphus Schrenkii Rupr. Root[J].Liaoning Journal of Traditional Chinese Medicine,2007,34(11):1616-1617. |
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| Authors: | ZHANG Qing-gao HAN Rong-bi Liu Dong-mei WU Xue |
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| Institution: | Yanbian University, Yanji 133002 ,Jilin, China |
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| Abstract: | Objective:To study the chemical constituents of Philadelphus schrenkii Rupr.root.Methods:Wet distillation was applied to the research of volatile component,then the volatile component was extracted by ether and identified by GC-MS.Gel column chromatography and prepared TLC were used here to separate the non-volatile chemical constituents which were identified by NMR,MS,IR,UV and NOESY spectra.Results:Eight essential oils constituents and two compounds were got here.The two compounds are 4-hydroxy-3-methoxybenzyaldehyde and 7-hydroxy-8-methoxycoumarin.Conclusion:The essential oils constituents and the two compounds reported here are obtained from Philadelphus schrenkii Rupr.root for the first time. |
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| Keywords: | Philadelphus schrenkii Rupr 4-hydroxy-3-methoxybenzyaldehyde 7-hydroxy-8-methoxycoumarin essential oils |
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