| 千山活血膏质量标准研究 |
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| 引用本文： | 傅欣彤,李琰 ,杜小伟,张小茜,石任兵.千山活血膏质量标准研究[J].中国中药杂志,2006,31(17):1431-1433. |
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| 作者姓名： | 傅欣彤 李琰 杜小伟 张小茜 石任兵 |
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| 作者单位： | 1. 北京市药品检验所,北京,100035
2. 北京中医药大学,中药学院,北京,100102 |
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| 摘 要： | 目的：建立千山活血膏的鉴别及含量测定方法。方法：采用薄层色谱法鉴别三七、血竭，HPLC测定三七中人参皂苷Rg1的含量。结果：人参皂苷Rg1在0.153 9～1.026 0 μg 线性关系良好，平均回收率为97.5%，RSD为2.1%。结论：该方法简便易行，重复性好。
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| 关 键 词： | 千山活血膏 薄层色谱 血竭 三七 人参皂苷Rg1 HPLC |
| 文章编号： | 1001-5302（2006）17-1431-03 |
| 收稿时间： | 1/2/2005 12:00:00 AM |
| 修稿时间： | 2005-01-02 |
Study of quality standards on Qianshan Huoxue plaster |
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| FU Xin-tong ;LI Yan ;DU Xiao-wei ;ZHANG Xiao-qian ;SHI Ren-bing.Study of quality standards on Qianshan Huoxue plaster[J].China Journal of Chinese Materia Medica,2006,31(17):1431-1433. |
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| Authors: | FU Xin-tong ;LI Yan ;DU Xiao-wei ;ZHANG Xiao-qian ;SHI Ren-bing |
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| Institution: | 1. Beijing Municipal Institute for Drug Control, Beijing 100035, China; 2. Beijing University of Chinese Medicine, Beijing 100102, China |
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| Abstract: | OBJECTIVE: To establish the methods of identification and assay in Qianshan Huoxue Gao. METHOD: Using TLC to identify Sanchi, Dragon's Blood and using HPLC to determine the content of ginsenoside Rg1. RESULT: The linear range of ginsenoside Rg1 was from 0.153 9 to 1.026 microg. The average recovery was 97.4%, RSD was 2.1%. CONCLUSION: The methods are simple and have good reproducibility. |
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| Keywords: | Qianshan Huoxue plaster TLC notoginseng Daemonorops draco ginsenoside Rg1 HPLC |
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