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气相色谱法测定中毒样品中立克命含量的探讨
引用本文:谷日旭,王雁卿.气相色谱法测定中毒样品中立克命含量的探讨[J].山西职工医学院学报,2003,13(1):1-2.
作者姓名:谷日旭  王雁卿
作者单位:山西省疾病预防控制中心,山西,太原,030012
摘    要:目的:探讨了采用气相色谱法测定中毒样品中立克命的应用效果。方法:用二氯甲烷提取中毒样品中的立克命,经5%SE—30细口径玻璃填充色谱柱分离,氢火焰离子化检测器检测.采用气相色谱法快速测定。结果与结论:本法灵敏度高,干扰少,线性范围、精密度、准确度等实验结果均符合实验要求。

关 键 词:气相色谱法  测定  中毒样品  立克命  含量
文章编号:1671-0126(2003)01-0001-02
修稿时间:2002年11月7日

Determination of Coumatetralyl Content in Toxic Sample by Gas Chromatography
GU Ri-xu,WANG Yan-qing.Determination of Coumatetralyl Content in Toxic Sample by Gas Chromatography[J].Journal of Shanxi Medical College For Continuing Education,2003,13(1):1-2.
Authors:GU Ri-xu  WANG Yan-qing
Abstract:Objective: To investigate the application of gas chromatography in determing coumatetralyl in toxic samples.Methods: Coumatetralyl in toxic samples was extracted by dichloromethane,separated by 5%SE-30 glass column of small inner diameter,detected by flame ionisation detector and determined by gas chromatography.Results and Conclusion: This techninque is of high sensitivity and very little interference.The results,such as the linear range,precision and accuracy,meet experimental requirements.
Keywords:coumatetralyl  gas chromatography  toxic sample
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