| 毓麟合剂的HPLC指纹图谱研究 |
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| 引用本文： | 张玉萱,年华,徐玲玲,TAO Jiansheng,HUANG Baokang.毓麟合剂的HPLC指纹图谱研究[J].内蒙古中医药,2009,28(2). |
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| 作者姓名： | 张玉萱 年华 徐玲玲 TAO Jiansheng HUANG Baokang |
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| 作者单位： | 岳阳中西医结合医院药剂科,200437 |
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| 基金项目： | 上海中医药大学附属岳阳中西医结合医院院内课题 |
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| 摘 要： | 目的:采用HPLC建立毓麟合剂的指纹图谱测定方法。方法:采用ZORBAXSB-C18柱(4.6×150mm,5μm)色谱柱,甲醇-0.01mol/L盐酸水溶液为流动相进行梯度洗脱,流速0.5mL/min,检测波长250nm。结果:建立了毓麟合剂的HPLC对照指纹图谱,共检出14个分离度良好的共有峰。结论:所选择的10批毓麟合剂指纹图谱具有良好的相似性,该方法可靠、简便,可作为毓麟合剂质量控制的参考方法。
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| 关 键 词： | 毓麟合剂 质量控制 指纹图谱 HPLC |
HPLC FingerPrints of Yu-Lin mixture |
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| ZHANG Yuxuan,NIAN Hua,XU Lingling,TAO Jiansheng,HUANG Baokang.HPLC FingerPrints of Yu-Lin mixture[J].Nei Mongol Journal of Traditional Chinese Medicine,2009,28(2). |
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| Authors: | ZHANG Yuxuan NIAN Hua XU Lingling TAO Jiansheng HUANG Baokang |
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| Institution: | 1; TAO Jian-sheng2; HUANG Bao-kang3 (1.Department of Pharmacy; Yueyang Hospital of Chinese Integrative Medicine; Shanghai 200437; 2.Faculty of Pharmaceutics; Shanghai University of Traditional Chinese Medicine; Shanghai 201203; 3. Department of Pharmacognosy; School of Pharmacy; Second Military Medical University; Shanghai 200433); |
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| Abstract: | AIM:To set up the fingerprint chromatograms of Yu-Lin mixture by HPLC.METHODS:The chromatographic seperation was performed on an ZORBAX SB-C18 column(4.6×150mm,5μm)with a mobile phase consisting of methanol-0.01 mol/L hydrochloric acid water,gradient eluent,at the flow rate of 0.5 mL/min,detection wavelength was set at 250 nm.RESULT: Set up the fingerprint chromatograms of Yu-Lin mixture by HPLC,we have pinpointed 14 common peaks.CONCLUTION:There are good similarities among 10 batches of Yu-Lin mixture,and ... |
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| Keywords: | HPLC |
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