| 大孔吸附树脂富集雷公藤内酯醇的研究 |
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| 引用本文： | 王曙东,滕英博,谢虞昇,李克.大孔吸附树脂富集雷公藤内酯醇的研究[J].医学研究生学报,2005,18(3):204-205. |
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| 作者姓名： | 王曙东 滕英博 谢虞昇 李克 |
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| 作者单位： | 1. 南京军区总医院制剂科,江苏南京,210002
2. 南京军区总医院检验科,江苏南京,210002 |
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| 摘 要： | 目的：应用大孔吸附树脂D101型分离、纯化雷公藤内酯醇。方法：用醇提水沉后，经D101树脂吸附及氧化铝柱除杂，用95％乙醇解吸，高压液相色谱(HPLC)测定含量。结果：雷公藤内酯醇可得到较好的保留。结论：D101可应用于雷公藤内酯醇的富集。
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| 关 键 词： | 雷公藤内酯醇 大孔吸附树脂 高效液相色谱法 |
| 文章编号： | 1008-8199(2005)03-0204-02 |
| 修稿时间： | 2004年6月18日 |
Study on macroporous adsorbing resin for purification of triptolide |
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| WANG Shu-dong,TENG Ying-bo,XIE Yu-sheng,LI Ke.Study on macroporous adsorbing resin for purification of triptolide[J].Bulletin of Medical Postgraduate,2005,18(3):204-205. |
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| Authors: | WANG Shu-dong TENG Ying-bo XIE Yu-sheng LI Ke |
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| Institution: | WANG Shu-dong1,TENG Ying-bo1,XIE Yu-sheng1,LI Ke2 |
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| Abstract: | Objective: To apply D101 macroporous resin for separation and purification of triptolide. Methods: After extracted by alcohol the extracts were dissolved in water and passed through a macroporous resin column and a aluminum oxide column. Then the triptolide on the columns were eluated with 95% alcohol and determination by HPLC. Results:Triptolide could be retained on D101 column. Conclusion: D101 resin can be used to refine the triptolide. |
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| Keywords: | Triptolide Macroporous resin HPLC |
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