| 柴辛鼻敏康颗粒的质量标准研究 |
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| 引用本文： | 王晓飞,葛海生,于玲,柴江平.柴辛鼻敏康颗粒的质量标准研究[J].中国药房,2011(19):1800-1802. |
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| 作者姓名： | 王晓飞 葛海生 于玲 柴江平 |
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| 作者单位： | 中国人民武装警察部队药品仪器检验所;中国中医科学院广安门医院; |
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| 摘 要： | 目的:建立柴辛鼻敏康颗粒的质量标准。方法:采用薄层色谱(TLC)法对方中柴胡、细辛进行定性鉴别;采用高效液相色谱法对芍药苷进行含量测定。结果:TLC斑点清晰、易于识别、重复性好;芍药苷进样量在0.512～15.360μg范围内与峰面积积分值呈良好线性关系(r=0.9998),平均回收率为99.87%,RSD=0.97%(n=6)。结论:该质量控制方法简单、准确度高、专属性强,可有效控制柴辛鼻敏康颗粒的质量。
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| 关 键 词： | 柴辛鼻敏康颗粒 质量标准 薄层色谱法 高效液相色谱法 芍药苷 |
Quality Standard of Chaixin Biminkang Granules |
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| WANG Xiao-fei,GE Hai-sheng,YU Ling CHAI Jiang-ping.Quality Standard of Chaixin Biminkang Granules[J].China Pharmacy,2011(19):1800-1802. |
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| Authors: | WANG Xiao-fei GE Hai-sheng YU Ling CHAI Jiang-ping |
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| Institution: | WANG Xiao-fei,GE Hai-sheng,YU Ling(Institute for Drug Control,Chinese People＇s Armed Police Forces,Beijing 102613,China) CHAI Jiang-ping(Guang’anmen Hospital,China Academy of Chinese Medical Sciences,Beijing 100053,China) |
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| Abstract: | OBJECTIVE：To establish the quality standards of Chaixin biminkang granules. METHODS：TLC was adopted to identify Bupleuri Radix and Radix Et Rhizoma. HPLC method was used to test the content of paeoniflorin. RESULTS：TLC spots were clear,distinguished and reproducible. The linear range of paeoniflorin was 0.512～15.360 μg（r=0.999 8） with an average recovery of 99.87%（RSD=0.97%,n=6） . CONCLUSION：The method is simple,precise and specific and has good effect on quality control of Chaixin biminkang granules. |
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| Keywords: | Chaixin biminkang granule Quality standard TLC HPLC Paeoniflorin |
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