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不同产地木香挥发油成分的GC-MS分析比较
引用本文:陈飞龙,谭晓梅,汤庆发,邢学锋. 不同产地木香挥发油成分的GC-MS分析比较[J]. 中国药房, 2011, 0(23): 2187-2189
作者姓名:陈飞龙  谭晓梅  汤庆发  邢学锋
作者单位:南方医科大学中医药学院广东省中药制剂研究重点实验室;
摘    要:目的:比较不同产地木香药材中挥发油的含量和化学成分的差异。方法:采用水蒸气蒸馏法提取7批不同产地木香的挥发油,用气相色谱-质谱(GC-MS)联用法对挥发油进行化学成分的分析鉴定,用面积归一化法获得各化合物的相对百分含量。结果:药材中挥发油含量分别为0.8%~2.1%,从挥发油中共鉴定了46种化学成分,不同产地木香挥发油的主要成分组成均为内酯类、萜类化合物,但相对含量存在一定的差异。结论:用该方法能为木香药材的质量鉴别提供较好的依据。

关 键 词:木香  不同产地  挥发油  气相色谱-质谱联用法

GC-MS Analysis of Volatile Oil from Aucklandia lappa from Different Producing Areas
CHEN Fei-long,TAN Xiao-mei,TANG Qing-fa,XING Xue-feng. GC-MS Analysis of Volatile Oil from Aucklandia lappa from Different Producing Areas[J]. China Pharmacy, 2011, 0(23): 2187-2189
Authors:CHEN Fei-long  TAN Xiao-mei  TANG Qing-fa  XING Xue-feng
Affiliation:CHEN Fei-long,TAN Xiao-mei,TANG Qing-fa,XING Xue-feng(School of Traditional Chinese Medicine,Southern Medical University & Guangdong Provincial Key Laboratory of Traditional Chinese Medicine Preparation,Guangzhou 510515,China)
Abstract:OBJECTIVE:To compare the contents of volatile oil from Aucklandia lappa from different producing areas and the difference of chemical components.METHODS:The volatile oil was extracted from A.lappa by water distillation method.The chemical components of volatile oil were identified by GC-MS,and the relative contents of these constituents were calculated using peak area normalization method.RESULTS:The contents of volatile oil were 0.8%~2.1%.46 chemical components of volatile oil were identified.The main components of volatile oil were lactones and terpenes,but there was a little difference in relative contents.CONCLUSION:The method can be applied to identify the quality of A.lappa.
Keywords:Aucklandia lappa  Different producing areas  Volatile oil  GC-MS  
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