| 斑蝥炮制前后脂肪酸成分的GC-MS分析 |
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| 引用本文： | 刘沁,陈建伟,武露凌,李祥.斑蝥炮制前后脂肪酸成分的GC-MS分析[J].中国药房,2011(19):1788-1789. |
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| 作者姓名： | 刘沁 陈建伟 武露凌 李祥 |
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| 作者单位： | 南京中医药大学药学院;江苏省中药炮制重点实验室;江苏省体育科学研究所; |
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| 基金项目： | 江苏省中药炮制重点实验室开放式课题(ZYPZ006); 江苏省高校自然科学研究计划项目(02KJB360004) |
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| 摘 要： | 目的:分析斑蝥炮制前后脂肪酸组成。方法:石油醚提取斑蝥脂肪油,甲酯化处理后采用气相色谱-质谱联用技术分析化合物组成,用峰面积归一化法确定各成分相对含量。结果:从炮制前后的斑蝥脂肪油中共分离鉴定出10种脂肪酸成分,脂肪酸组成以油酸、硬脂酸、亚油酸为主。结论:炮制对斑蝥脂肪酸组成影响不大。本试验可为斑蝥炮制前后的成分研究提供理论依据。
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| 关 键 词： | 斑蝥 炮制 脂肪酸 气相色谱-质谱联用技术 |
GC-MS Analysis of Fatty Acids from Mylabris before and after Processing |
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| LIU Qin,CHEN Jian-wei,LI Xiang CHEN Jian-wei,LI Xiang WU Lu-ling.GC-MS Analysis of Fatty Acids from Mylabris before and after Processing[J].China Pharmacy,2011(19):1788-1789. |
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| Authors: | LIU Qin CHEN Jian-wei LI Xiang CHEN Jian-wei LI Xiang WU Lu-ling |
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| Institution: | LIU Qin,CHEN Jian-wei,LI Xiang(College of Pharmacy,Nanjing University of Traditional Chinese Medicine,Nanjing 210046,China) CHEN Jian-wei,LI Xiang(Jiangsu Key Laboratory for Chinese Materia Medica Processing,Nanjing 210029,China) WU Lu-ling(Jiangsu Institute of Sports Science Research,Nanjing 210014,China) |
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| Abstract: | OBJECTIVE:To analyze the chemical constituents of the fatty acids from Mylabris before and after processing. METHODS:The fatty oil of Mylabris was extracted by petroleum ether and analyzed by GC-MS after methyl esterifying. The content of chemical components was determined by peak area normalization method. RESULTS:10 kinds of fatty acid were isolated from preprocessed Mylabris fatty oil and processed Mylabris fatty oil. Main chemical constituents of fatty acid were oleic acid,oleic acid and linoleic acid. ... |
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| Keywords: | Mylabris Processing Fatty acids GC-MS |
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