| 秦岭翠雀花化学成分的研究 |
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| 引用本文： | 何仰清,马占营,杨谦,高黎明,田萍,杜宝中. 秦岭翠雀花化学成分的研究[J]. 中国药学杂志, 2009, 44(6): 415-417 |
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| 作者姓名： | 何仰清 马占营 杨谦 高黎明 田萍 杜宝中 |
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| 作者单位： | 1.西安理工大学应用化学系 西安 710054;2.咸阳师范学院化学系 陕西咸阳 721000;3.西北师范大学化学化工学院 兰州 7300700 |
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| 基金项目： | 西安理工大学科研创新项目资助(108-2005) |
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| 摘 要： | 目的对秦岭翠雀花(Delphinium giraldii)进行化学成分研究。方法采用硅胶柱色谱进行分离纯化,根据化合物的理化性质和波谱数据鉴定结构。结果从秦岭翠雀花的氯仿部位分离得到8个化合物,分别鉴定为3-acetylaconitine(Ⅰ),mesaconitine(Ⅱ),benzoylaconitine(Ⅲ),delelatine(Ⅳ),siwanineA(Ⅴ),methyllycaconitine(Ⅵ),β-谷甾醇(Ⅶ)和胡萝卜苷(Ⅷ)。结论化合物1～4首次从该植物中分离得到。
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| 关 键 词： | 翠雀属 秦岭翠雀花 二萜生物碱 |
| 收稿时间： | 2008-05-10; |
Study on Chemical Constituents of Delphinium giraldii |
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| HE Yang-qing,MA Zhan-ying,YANG Qian,GAO Li-ming,TIAN Ping,DU Bao-zhong. Study on Chemical Constituents of Delphinium giraldii[J]. Chinese Pharmaceutical Journal, 2009, 44(6): 415-417 |
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| Authors: | HE Yang-qing MA Zhan-ying YANG Qian GAO Li-ming TIAN Ping DU Bao-zhong |
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| Affiliation: | 1. Department of Applied Chemistry,Xi′an University of Technology,Xi′an 710054,China;2. Department of Chemistry,Xianyang Normal University,Xianyang 712000,China;3. Department of Chemistry,Key Laboratory of Polymer Materials of Gansu Province,Northwest Normal University,Lanzhou 730070,China |
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| Abstract: | OBJECTIVE To study the chemical constituents from Delphinium giraldii. METHODS The whole of this plants were extracted three times with 90% EtOH at the room temperature. The ethanol extracts were combined and concentrated under reduced pressure at 65 ℃ to yield residue,which was suspended in water and successively partitioned with light petroleum and chloroform. The chloroform extraction was isolated and purified by silica gel column chromatography. The structures were elucidated by their physiochemical characteristics and spectral data. RESULTS Eight compounds were isolated and elucidated as 3-acetylaconitine (Ⅰ ),mesaconitine (Ⅱ ),benzoylaconitine (Ⅲ ),delelatine(Ⅳ),siwanine A (Ⅴ ) ,methyllycaconitine (Ⅵ ),β-sitosterol (Ⅶ ) and daucosterol (Ⅷ ). CONCLUSION Compound Ⅰ,Ⅱ,Ⅲ and Ⅳ were obtained from Delphinium giraldii for the first time. |
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| Keywords: | Delphinium')" href=" #" >Delphinium giraldii')" href=" #" > Delphinium giraldii diterpene alkaloids |
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