| HPLC法同时测定小儿平喘祛痰颗粒中盐酸麻黄碱、盐酸伪麻黄碱、苦杏仁苷含量 |
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| 引用本文： | 杨德斌,仝燕,马振山,王琳,董美虹,李艳玲,王锦玉.HPLC法同时测定小儿平喘祛痰颗粒中盐酸麻黄碱、盐酸伪麻黄碱、苦杏仁苷含量[J].中国中药杂志,2013,38(5):687-690. |
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| 作者姓名： | 杨德斌 仝燕 马振山 王琳 董美虹 李艳玲 王锦玉 |
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| 作者单位： | 1. 中国中医科学院中药研究所,北京100700;天津中医药大学,天津300193
2. 中国中医科学院中药研究所,北京,100700 |
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| 基金项目： | 中国中医科学院基本科研业务费自主选题项目(2011XYCZ-07) |
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| 摘 要： | 目的:建立同时测定小儿平喘祛痰颗粒中3种成分含量的高效液相色谱法.方法:采用Phenyl Ether色谱柱(4.6 mm ×250 mm,5μm),流动相乙腈-0.1％磷酸溶液(含0.1％的三乙胺)(3∶97),紫外检测波长210 nm,流速1.0 mL·min-,柱温35℃.结果:盐酸麻黄碱、盐酸伪麻黄碱、苦杏仁苷的线性范围分别为0.078 60 ～3.144 μg(r=1.000 0),0.103 4～2.068 μg(r =0.999 7),0.430 5～3.157 μg(r =0.999 8)；平均回收率分别为98.46％ (RSD 1.1％),103.0％ (RSD1.5％),97.15％ (RSD2 1％).结论:该法简便、稳定、可靠,可以用于小儿平喘祛痰颗粒中盐酸麻黄碱、盐酸伪麻黄碱、苦杏仁苷的含量测定.
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| 关 键 词： | 高效液相色谱 小儿平喘祛痰颗粒 盐酸麻黄碱 盐酸伪麻黄碱 苦杏仁苷 |
| 收稿时间： | 7/6/2012 12:00:00 AM |
Simultaneous determination of ephedrine hydrochloride, D-pseudo-ephedrine and amygdalin in Xiao'er Pingchuan Qutan granule by HPLC |
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| YANG De-bin,TONG Yan,MA Zhen-shan,WANG Lin,DONG Mei-hong,LI Yan-ling and WANG Jin-yu.Simultaneous determination of ephedrine hydrochloride, D-pseudo-ephedrine and amygdalin in Xiao'er Pingchuan Qutan granule by HPLC[J].China Journal of Chinese Materia Medica,2013,38(5):687-690. |
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| Authors: | YANG De-bin TONG Yan MA Zhen-shan WANG Lin DONG Mei-hong LI Yan-ling and WANG Jin-yu |
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| Institution: | Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China;Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China |
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| Abstract: | |
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| Keywords: | HPLC Xiao'er Pingchuan Qutan granule ephedrine hydrochloride D-pseudo-ephedrine amygdalin |
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