| 薄层色谱扫描法测定芪黄通秘软胶囊中黄芪甲苷的含量 |
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| 引用本文： | 孔德宪,刘育强,赵伯友,李香梅,陈浩达,卢树杰.薄层色谱扫描法测定芪黄通秘软胶囊中黄芪甲苷的含量[J].亚太传统医药,2011,7(6):18-19. |
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| 作者姓名： | 孔德宪 刘育强 赵伯友 李香梅 陈浩达 卢树杰 |
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| 作者单位： | 1. 神威药业有限公司,河北石家庄,051430
2. 神威药业有限公司,河北石家庄051430;河北省中药注射剂工程技术研究中心,河北石家庄051430 |
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| 摘 要： | 目的:建立芪黄通秘软胶囊中黄芪甲苷含量的测定方法。方法:薄层色谱扫描法,测定波长λS=530nm,参比波长λR=700nm,展开剂为氯仿-甲醇-水(13:6:2)。结果:黄芪甲苷在1.00～5.00μg范围内呈良好线性关系,平均回收率为98.7%,RSD=2.26%。结论:该方法简便、灵敏、重现性好,可用于芪黄通秘软胶囊中黄芪甲苷含量的测定。
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| 关 键 词： | 芪黄通秘软胶囊 薄层色谱扫描法 黄芪甲苷 |
Content Determination of Astragaloside A in Qihuangtongmi Capsules by TLC Scanning |
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| Kong Dexian,Liu Yuqiang,Zhao Boyou,Li Xiangmei,Chen Haodal,Lu Shujie.Content Determination of Astragaloside A in Qihuangtongmi Capsules by TLC Scanning[J].Asia-Pacific Traditional Medicine,2011,7(6):18-19. |
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| Authors: | Kong Dexian Liu Yuqiang Zhao Boyou Li Xiangmei Chen Haodal Lu Shujie |
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| Institution: | Kong Dexian1,Liu Yuqiang1,Zhao Boyou1,Li Xiangmei1,Chen Haoda1 Lu Shujie1,2(1.Shineway Pharmaceutical Co ltd.,Shijiazhuang 051430,China,2.Hebei Province Engineering Research Center for Traditional Chinese drug Injections,China) |
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| Abstract: | Objective：To determine the content of astragaloside A in Qihuangtongmi Capsules.Methods：TCL scanning method was used.Detection wavelength：λS=530nm,Reference wavelength：λR=700nm.The mobile phase was chloroform-methanol-water（13∶6∶2）.Results：A good linear range was shown at the concentration from 1.00μg to 5.00μg.The average recovery was 98.7% and the RSD was 2.94%.Conclusion：The method is simple,sensitive,reproducible and can be used for the quality control of Qihuangtongmi Capsules. |
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| Keywords: | Qihuangtongmi Capsules TCL Scanning Astragaloside A |
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