| 多指标综合评分法优选意大利牛舌草总黄酮的提取工艺 |
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| 引用本文： | 路文杰,程雪梅,滕亮,马桂芝. 多指标综合评分法优选意大利牛舌草总黄酮的提取工艺[J]. 上海中医药杂志, 2016, 50(12): 89-93 |
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| 作者姓名： | 路文杰 程雪梅 滕亮 马桂芝 |
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| 作者单位： | 新疆医科大学药学院,新疆乌鲁木齐,830011,上海中医药大学中药研究所,中药标准化教育部重点实验室,中药新资源与质量标准综合评价国家中医药管理局重点研究室,上海中药标准化研究中心,上海,201210,新疆医科大学第一附属医院药学部,新疆乌鲁木齐,830011;新疆医科大学第一附属医院昌吉分院,新疆昌吉,831100,新疆医科大学药学院,新疆乌鲁木齐,830011 |
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| 基金项目： | 新疆维吾尔自治区科技计划资助项目(20113015-2) |
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| 摘 要： | 目的优选意大利牛舌草总黄酮的提取工艺。方法以总黄酮提取率、芦丁提取率及出膏率为考察指标,采用两种多指标综合评分法及L9(34)重复正交试验设计,优选意大利牛舌草回流提取法的工艺条件。结果用于测定提取物中总黄酮含量与芦丁含量的测定方法均符合方法学要求。意大利牛舌草总黄酮回流提取法优选工艺条件为:料液比1∶20;提取温度100℃;乙醇体积分数75%;提取2次,每次2 h。结论验证试验表明优选出的提取工艺简便、合理、可行,为后续研究奠定了基础。
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| 关 键 词： | 意大利牛舌草 回流提取法 多指标综合评分 重复正交试验设计 |
| 收稿时间： | 2016-09-08 |
Optimization of extraction process of total flavonoids from Anchusa italica Retz. by multi-index comprehensive score method |
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| LU Wen-jie,CHENG Xue-mei,TENG Liang and MA Gui-zhi. Optimization of extraction process of total flavonoids from Anchusa italica Retz. by multi-index comprehensive score method[J]. Shanghai Journal of Traditional Chinese Medicine, 2016, 50(12): 89-93 |
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| Authors: | LU Wen-jie CHENG Xue-mei TENG Liang MA Gui-zhi |
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| Affiliation: | Pharmacy College,Xinjiang Medical University,Urumqi,830011,Institute of Traditional Chinese Medicine, Shanghai University of Traditional Chinese MedicineKey Laboratory of Education Ministry for Standardization of Traditional Chinese MedicineKey Laboratory of State Administration of Traditional Chinese Medicine for Comprehensive Evaluation of New Resources and Quality Standard of Traditional Chinese MedicineShanghai Research Center for Standardization of Traditional Chinese Medicine, Shanghai, 201210,Department of Pharmacy,The First Hospital Affiliated to Xinjiang Medical University, Urumqi,830011;Changji Branch Hospital,The First Hospital Affiliated to Xinjiang Medical University,Changji,831100 and Pharmacy College,Xinjiang Medical University,Urumqi,830011 |
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