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| 丝毛瑞香化学成分研究 | |
| 引用本文： | 陈玉琪,苏娟,沈云亨,张薇,扈晓佳,许文争,张卫东,孔令义.丝毛瑞香化学成分研究[J].中国药学杂志,2008,43(19):1453-1456. |
| 作者姓名： | 陈玉琪 苏娟 沈云亨 张薇 扈晓佳 许文争 张卫东 孔令义 |
| 作者单位： | 1. 中国药科大学天然药化教研室,南京,210009;第二军医大学药学院天然药化教研室,上海,200433 2. 第二军医大学药学院天然药化教研室,上海,200433 3. 上海交通大学药学院,上海,200030 4. 第二军医大学药学院天然药化教研室,上海,200433;上海交通大学药学院,上海,200030 5. 中国药科大学天然药化教研室,南京,210009 |
| 摘 要： | 目的研究丝毛瑞香的化学成分。方法利用反复硅胶柱色谱、凝胶柱色谱进行分离,通过波谱解析和理化性质进行化合物结构鉴定。结果分离得到10个苯丙素类化合物,分别鉴定为双白瑞香素(1),瑞香新素(2),5′-去甲氧基瑞香新素(3),(-)-双氢芝麻素(4),丁香树脂酚(5),芥子醛(6),edgeworin(7),edgeworthin(8),(-)-epinortrachelogenin(9)和落叶松脂醇(10)。结论化合物9为首次从瑞香科植物中分离所得,其余均为从该植物中首次分离得到。 |
| 关 键 词： | 丝毛瑞香 化学成分 苯丙素类 |
| 收稿时间： | 2007-12-28; |
Studies on Chemical Constituents of Daphne holosericea(Diels)Hamaya |
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| CHEN Yu-qi,SU Juan,SHEN Yun-heng,ZHANG Wei,HU Xiao-jia,XU Wen-zheng,ZHANG Wei-dong,KONG Ling-yi.Studies on Chemical Constituents of Daphne holosericea(Diels)Hamaya[J].Chinese Pharmaceutical Journal,2008,43(19):1453-1456. | |
| Authors: | CHEN Yu-qi SU Juan SHEN Yun-heng ZHANG Wei HU Xiao-jia XU Wen-zheng ZHANG Wei-dong KONG Ling-yi |
| Institution: | 1.Department of Natural Medicinal Chemistry，China Pharmaceutical University，Nanjing 210009，China； 2. Department of Phytochemistry，School of Pharmacy，Second Military Medical University，Shanghai 200433，China； 3. School of Pharmacy，Shanghai Jiao Tong University，Shanghai 200030，China |
| Abstract: | OBJECTIVE To investigate the chemical constituents of Daphne holosericea(Diels) Hamaya.METHODS The separation was obtained by repeated column chromatograph with silica gel and Sephadex LH-20.The structures were elucidated on the basis of spectral analysis and physical-chemical properties.The spectral data was compared with literature values.RESULTS Ten phenylpropanoids were isolated and identified as daphnoretin(1),daphneticin(2),5'-demethoxydaphneticin(3),(-)-dihydrosesamin(4),syringaresinol(5),sinapaldehyde(6),edgeworin(7),edgeworthin(8),(-)-epinortrachelogenin(9) and lariciresinol(10).CONCLUSION Compound 9 was first obtained from the plants of Thymelaeaceae,while the others were isolated from this plant for the first time. |
| Keywords: | Daphne holosericea chemical constituents phenylpropanoids |
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