| UPLC法同时测定十八味诃子利尿丸中4种药效成分含量的方法研究 |
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| 引用本文： | 杨凤梅,张幸福,张炜,范莹莹. UPLC法同时测定十八味诃子利尿丸中4种药效成分含量的方法研究[J]. 青海医学院学报, 2011, 32(1): 53-59 |
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| 作者姓名： | 杨凤梅 张幸福 张炜 范莹莹 |
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| 作者单位： | 青海省药品检验所 |
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| 摘 要： | 目的 建立同时测定十八味诃子利尿丸中羟基红花黄色素A、姜黄素、盐酸小檗碱和没食子酸含量的方法.方法 基于HPLC法,利用这4种成分的极性大小,和在一个色谱系统上的保留时间不同,考证不同流动相组合和梯度比例.通过UPLC法转换测定波长同时测定十八味诃子利尿丸4种药效成分的含量.结果 此方法所测4种成分羟基红花黄色素A、姜...
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| 关 键 词： | 十八味诃子利尿丸 羟基红花黄色素A 姜黄素 盐酸小檗碱 没食子酸 UPLC |
DETERMINATION OF FOUR EFFICACY COMPONENTS IN SHIBAWEI HEZILINIAO PILL BY UPLC |
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| Yang Fengmei,Zhang Xingfu,Zhang Wei,Fan Yingying. DETERMINATION OF FOUR EFFICACY COMPONENTS IN SHIBAWEI HEZILINIAO PILL BY UPLC[J]. Journal of Qinghai Medical College, 2011, 32(1): 53-59 |
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| Authors: | Yang Fengmei Zhang Xingfu Zhang Wei Fan Yingying |
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| Affiliation: | Yang Fengmei,Zhang Xingfu,Zhang Wei,Fan Yingying (Qinghai Provincial Insitute for Drug control) |
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| Abstract: | Objective To establish the simultaneous determination methods for hydroxysafflor yellow A curcumin berberine hydrochloride and gallic acid in Shibawei Heziliniao Pill is reported.Methods Based on HPLC,use this four ingredients polarity size,and in a chromatographic retention time on the system is different form research in different ratio of mobile phase composition and gradient.Wavelength conversion by UPLC method simultaneously detected in four efficacy components of shibawei heziliniao pill.Results The h... |
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| Keywords: | UPLC |
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