| 高效液相色谱法测定安乃近含量 |
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| 引用本文： | 宁美英,李青山. 高效液相色谱法测定安乃近含量[J]. 临床医药实践, 2000, 9(7) |
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| 作者姓名： | 宁美英 李青山 |
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| 作者单位： | 1. 太原市传染病医院,山西,太原,030012
2. 山西医科大学,山西,太原,030001 |
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| 摘 要： | 目的 :建立以高效液相色谱法测定安乃近的含量。方法 :以 C1 8为固定相 ,甲醇 :水 ( 80∶ 2 0 )为流动相 ,氨基比林为内标物 ,检测波长为 2 5 4m m,甲醇溶液及水溶液放置考察其稳定性。结果 :平均回收率± RSD为 10 0 .2 %± 0 .0 6 % ( n=6 ) ,安乃近在甲醇溶液中稳定 ,在水溶液中放置易氧化。结论 :方法简便 ,快速经济 ,专属性强
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| 关 键 词： | 高效液相色谱法 安乃近 稳定性 |
Determination of Analgin by HPLC |
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| NING Mei-ying,LI Qing-shan. Determination of Analgin by HPLC[J]. Proceeding of Clinical Medicine, 2000, 9(7) |
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| Authors: | NING Mei-ying LI Qing-shan |
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| Abstract: | Objective:HPLC determination of Analgin and its stability.Method:Using Aminoantiprine as internal standard, detection was at 254mm,column was C 18 ,mobile phase was methyl:H 2O(80∶20),the methyl solution and water solution was studied.Results:Average recovery was 100.2%±0.06%(X±RSD,n=6).Conclusion:the method is simple and specific and economic. |
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| Keywords: | HPLC analgin stability |
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