| HPLC法测定通窍鼻炎片中5-O-甲基维斯阿米醇苷的含量 |
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| 引用本文： | 李爱玲,宫瑞萍. HPLC法测定通窍鼻炎片中5-O-甲基维斯阿米醇苷的含量[J]. 齐鲁药事, 2006, 25(4): 222-223 |
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| 作者姓名： | 李爱玲 宫瑞萍 |
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| 作者单位： | 1. 山东药品食品职业学院,淄博,255011
2. 山东华洋制药有限公司,淄博,255190 |
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| 摘 要： | 目的建立高效液相色谱法测定通窍鼻炎片中5-O-甲基维斯阿米醇苷的含量。方法Kromassil C18色谱柱,5μm,250×4.6mm,甲醇-水-四氢呋喃(38∶62∶1)为流动相,流速为1.0ml.min-1,检测波长254nm。结果本法线性关系良好(r=0.9998)。平均加样回收率100.07%,RSD=1.39%(n=5)。结论本法简便易行,结果准确,重现性好。可用于通窍鼻炎片的质量控制。
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| 关 键 词： | 通窍鼻炎片 高效液相色谱法 5-O-甲基维斯阿米醇苷 |
| 文章编号： | 1672-7738(2006)04-0222-02 |
Determination of 5-O-Methylvisammioside in Tongqiao Biyan Tablets by HPLC |
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| LI Ai-ling,GONG Rui-ping. Determination of 5-O-Methylvisammioside in Tongqiao Biyan Tablets by HPLC[J]. qilu pharmaceutical affairs, 2006, 25(4): 222-223 |
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| Authors: | LI Ai-ling GONG Rui-ping |
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| Abstract: | OBJECTIVE To establish a HPLC method for determination of 5-O-Methylvisammioside in Tongqiao Biyan Tablets.METHODS The Kromassil C_(18) column(5μm,250×4.6mm) was used,the mobile phase was methanol-water-tetrahydrofuran(38∶62∶1).Flow rate was 1.0ml·min~(-1).Detection wavelength was at 254nm.RESULTS The method had a good linear dependence(r=0.9998).The average recovery was 100.07%(RSD=1.39%,n=5).CONCLUSION The method is simple,rapid,accurate and reliable,and can be used to control quality of Tongqiao Biyan Tablets. |
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| Keywords: | Tongqiao Biyan Tablets HPLC 5-O-Methylvisammioside |
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