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| 艾纳香化学成分的研究 | |
| 引用本文： | 梁会,曹佩雪,邱净英,李霞,柴立,梁光义. 艾纳香化学成分的研究[J]. 时珍国医国药, 2011, 22(2): 308-309. DOI: 10.3969/j.issn.1008-0805.2011.02.019 |
| 作者姓名： | 梁会 曹佩雪 邱净英 李霞 柴立 梁光义 |
| 作者单位： | 1. 贵阳中医学院,贵州,贵阳,550025;贵州省中国科学院天然产物化学重点实验室,贵州,贵阳,550002 2. 贵州省中国科学院天然产物化学重点实验室,贵州,贵阳,550002 3. 贵州宏宇药业有限公司,贵州,贵阳,550018 |
| 基金项目： | 国家“973”计划前期研究专项(No.2007CB516813); 贵州省科技创新人才团队专项资金黔科合人才团队专项资金(No.[2008]4008); 贵州省重点实验室项目(黔科合计Z字[2009]4005) |
| 摘 要： | 目的研究艾纳香Blumea balsanaferaDC.的化学成分。方法采用硅胶柱色谱、薄层色谱、Sephadex LH-20柱色谱等方法分离纯化化合物,利用核磁共振等现代波谱技术解析化合物结构。结果从艾纳香的醋酸乙酯、氯仿部分分离得到7个化合物,鉴定为艾纳香素(blumeatin,1)、花椒油素(xanthoxylin,2)、木犀草素(luteolin,3)、胡萝卜苷(dau-costerol,4)、槲皮素(quercetin,5)、帕得马亭(padmatin,6)、3,5,5′,7-四羟基黄烷酮(3,5,5′,7-tetrahydroxyflavanone,7)。结论除化合物1和5外,其余5个化合物均为第1次从艾纳香中获得。 |
| 关 键 词： | 艾纳香 化学成分 黄酮 |
Study on the Chemical Constituents of Blumea balsanifera DC. |
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| LIANG Hui,CAO Pei-xue,QIU Jing-ying,LI Xia,CHAI Li,LIANG Guang-yi. Study on the Chemical Constituents of Blumea balsanifera DC.[J]. Lishizhen Medicine and Materia Medica Research, 2011, 22(2): 308-309. DOI: 10.3969/j.issn.1008-0805.2011.02.019 | |
| Authors: | LIANG Hui CAO Pei-xue QIU Jing-ying LI Xia CHAI Li LIANG Guang-yi |
| Affiliation: | LIANG Hui1,2,CAO Pei-xue2,QIU Jing-ying 2,LI Xia3,CHAI Li3,LIANG Guang-yi 2(1.Guiyang College of Traditional Chinese Medicine,Guizhou,Guiyang 550002 China,2.The Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Science,Guiyang,Guizhou 550002 China,3.Guizhou Holy Pharmaceutical Co.,Ltd.,Guiyang 550018 China) |
| Abstract: | Objective To study the chemical constituents of Blumea balsanifera DC.Methods The compounds were isolated and repeatedly purified by silica gel column chromatography,TLC,Sephadex LH-20 column chromatography,and their structures were elucidated on the basis of physico-chemical constants and spectral analysis.Results Seven compounds were obtained and elucidated as blumeatin(1),xanthoxylin(2),luteolin(3),daucosterol(4),quercetin(5),padmatin(6),3,5,5′,7-tetrahydroxyflavanone(7).Conclusion The compounds 2,3,4,6 and 7 were isolated from this genus for the first time. |
| Keywords: | Blumea balsanifera DC. Chemical studies Flavanoids |
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