| 蒲地蓝消炎片的质量标准研究 |
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| 引用本文： | 宋茹,迟归兵,袁继民. 蒲地蓝消炎片的质量标准研究[J]. 解放军药学学报, 2008, 24(3): 229-231 |
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| 作者姓名： | 宋茹 迟归兵 袁继民 |
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| 作者单位： | 济南军区药品仪器检验所,山东,济南,250022 |
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| 摘 要： | 目的完善蒲地蓝消炎片的质量控制方法。方法采用薄层色谱法对方中黄芩、蒲公英与苦地丁进行鉴别；用高效液相色谱法测定方中黄芩苷的含量。结果TLC鉴别方法专属性强；黄芩苷线性范围为0．12-3．0μg（r=0．9997），平均回收率为98．8％，RSD为0．7％（n=6）。结论本方法操作简便，结果准确，灵敏度高，重复性好。该质量标准可有效地控制蒲地蓝消炎片的质量。
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| 关 键 词： | 蒲地蓝消炎片 质量标准 TLC HPLC 黄芩苷 |
| 文章编号： | 1008-9926(2008)03-0229-03 |
| 修稿时间： | 2007-01-15 |
Study on Quality Standard of Pudilanxiaoyan Tablets |
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| SONG Ru,CHI Gui-Bing,YUAN Ji-Min. Study on Quality Standard of Pudilanxiaoyan Tablets[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2008, 24(3): 229-231 |
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| Authors: | SONG Ru CHI Gui-Bing YUAN Ji-Min |
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| Affiliation: | 1Institute for Drug and Instrument Control of the Jinan Military Region, Jinan 250022,Shandong China) |
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| Abstract: | Aim To consummate a method for quality control of Pudilanxiaoyan Tablets. Methods TLC was used for the identification of Radix Scutellariae, Herba Taraxaci and Herba Corydalis Bunge＇anae. HPLC was used for the determination of baicalin in Pudilanxiaoyan Tablets. Results The TLC identification was highly specific and the spots were clear. The linear range of baicalin was from 0.12 - 3.01μg, r = 0. 999 7. The average recovery of baicalin was 98.8%, RSD was 0.7%. Conclusion These methods were easy to operate with accurate results, high sensitivity and good reproducibility. The quality standard can effectively control the quality of Pudilanxiaoyan Tablets. |
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| Keywords: | Pudilanxiaoyan Tablets Quality standard TLC HPLC Baicalin |
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