| 穿黄消炎胶囊的质量控制研究 |
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| 引用本文： | 陶善斌,汪电雷.穿黄消炎胶囊的质量控制研究[J].安徽医药,2013,17(6):932-934. |
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| 作者姓名： | 陶善斌 汪电雷 |
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| 作者单位： | 安徽省芜湖县医院药剂科,安徽,芜湖,241100;安徽中医学院,安徽,合肥,230031 |
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| 摘 要： | 目的建立穿黄消炎胶囊的质量控制研究方法。方法采用薄层色谱法对穿黄消炎胶囊中的穿心莲和一只黄花进行定性鉴别;采用高效液相色谱测定脱水穿心莲内酯含量。结果薄层鉴别色谱特征明显,专属性强;脱水穿心莲内酯在12.92～129.20 mg.L-1范围内线性关系良好(r=0.999 7),平均加样回收率为99.52%(RSD=0.66%)。结论该方法准确、灵敏,重复性好,可作为穿黄消炎胶囊的质量控制研究。
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| 关 键 词： | 穿黄消炎胶囊 TLC HPLC 脱水穿心莲内酯 质量控制 |
A quality control research of Bao tai pills |
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| TAO Shan-bin,WANG Dian-lei.A quality control research of Bao tai pills[J].Anhui Medical and Pharmaceutical Journal,2013,17(6):932-934. |
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| Authors: | TAO Shan-bin WANG Dian-lei |
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| Institution: | 2 ( 1. Department of Pharmacy, Wuhu County Hospital, Wuhu,Anhui 241100,China;2. Department of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei,Anhui 230031, China) |
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| Abstract: | Objective To establish the method for the quality control research of Bao tai pills. Methods TLC was used to make a thin layer qualitative identification for Herba Andrographis and Soliclago decur in Bao tai pills. Determination content of Paeoniflorin in Bao tai pills was conducted by HPLC. Results The TLC identification chromatography showed obvious characteristics. Paeoniflorin had good lin- ear relationship in the concentration range of 12.92 - 129.20 mg ·L-5 （ r = 0.9997）. The average recovery, was 99.52% , and RSD was 0.66%. Conclusion The method is accurate,delicate and reproducible,which can be applied for the quality control research of Bao tai pills. |
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| Keywords: | Bao tai pills TLC HPLC Paeoniflorin quality control |
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