| HPLC法测定气血双补丸中黄芪甲苷的含量 |
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| 引用本文： | 杨群华,宫瑞萍,王庆忠.HPLC法测定气血双补丸中黄芪甲苷的含量[J].齐鲁药事,2008,27(12). |
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| 作者姓名： | 杨群华 宫瑞萍 王庆忠 |
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| 作者单位： | 1. 广东食品药品职业学院,广东,广州,510520
2. 山东华洋制药有限公司,山东,淄博255190 |
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| 摘 要： | 目的建立气血双补丸中黄芪甲苷的含量测定方法。方法采用高效液相色谱法,色谱柱为Inertex C18(100mm×4.6mm,5μm);流动相为乙腈-水(28∶72);流速1.0mL.min-1。结果平均回收率为99.59%,RSD为0.28%。结论此方法灵敏、准确、重复性好,其它组分对测定无干扰,可用于气血双补丸的质量控制。
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| 关 键 词： | 高效液相色谱法 气血双补丸 黄芪甲苷 含量 |
Determination of astragaloside in Qixueshuangbu Pill by HPLC |
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| YANG Qun-hua,GONG Rui-ping,WANG Qing-zhong.Determination of astragaloside in Qixueshuangbu Pill by HPLC[J].qilu pharmaceutical affairs,2008,27(12). |
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| Authors: | YANG Qun-hua GONG Rui-ping WANG Qing-zhong |
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| Institution: | YANG Qun-hua,GONG Rui-ping,WANG Qing-zhong1 |
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| Abstract: | OBJECTIVE To establish a method for the determination of astragaloside in Qixueshuangbu Pill.METHODS HPLC method was performed on column Inertex C18(100mm×4.6mm,5μm);acetonitrile-water(28∶72)as the mobil phase,the flowrate was 1.0mL·min-1.RESULTS The average recovery was 99.59%,with RSD 0.28%.CONCLUSION The method was sensitive,accurate and with a good reproducibility.This method can be used to control the quality of Qixueshuangbu Pill. |
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| Keywords: | HPLC Qixueshuangbu Pill astragaloside content |
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