| 复方驱虫斑鸠菊丸质量标准 |
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| 引用本文： | 古丽斯坦·阿吾提,何承辉,刘宣麟,薛桂蓬. 复方驱虫斑鸠菊丸质量标准[J]. 中国实验方剂学杂志, 2013, 19(13): 94-96 |
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| 作者姓名： | 古丽斯坦·阿吾提 何承辉 刘宣麟 薛桂蓬 |
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| 作者单位： | 新疆维吾尔自治区药物研究所,乌鲁木齐,830004 |
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| 基金项目： | 新疆维吾尔自治区重大科技专项(201130105-3) |
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| 摘 要： | 目的:建立复方驱虫斑鸠菊丸的质量控制方法.方法:采用显微鉴别法和薄层色谱法进行定性鉴别,高效液相色谱法测定样品中胡椒碱的含量.结果:显微鉴别特征明显；薄层色谱鉴别斑点清晰,专属性强；含量测定胡椒碱浓度在5.42～43.36mg·L-1呈良好线性关系,r=0.999 8(n=9),平均回收率100.72％,RSD 0.56％.结论:定性、定量方法简便、可靠、准确,可用于复方驱虫斑鸠菊丸的质量控制.
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| 关 键 词： | 复方驱虫斑鸠菊丸 显微鉴别 薄层鉴别 高效液相色谱 胡椒碱 |
| 收稿时间： | 2012-07-16 |
Quality Standard of Compound Quchongbanjiuju Pill |
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| Gulistan-Awuti,HE Cheng-hui,LIU Xuan-lin and XUE Gui-peng. Quality Standard of Compound Quchongbanjiuju Pill[J]. China Journal of Experimental Traditional Medical Formulae, 2013, 19(13): 94-96 |
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| Authors: | Gulistan-Awuti HE Cheng-hui LIU Xuan-lin XUE Gui-peng |
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| Affiliation: | Xinjiang Institute of Materia Medica, Urumqi 830004, China;Xinjiang Institute of Materia Medica, Urumqi 830004, China;Xinjiang Institute of Materia Medica, Urumqi 830004, China;Xinjiang Institute of Materia Medica, Urumqi 830004, China |
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| Abstract: | Objective:To establish the method for quality control of Compound Quchongbanjiuju Pills. Method: Thin-layer chromatography and microscopic identification were used to identify Compound Quchongbanjiuju Pills. The content of pepper alkali was determined by HPLC. Result: Characteristic of microscopical identification was obvious. The TLC identification was highly specific and spots were clear. There was good linearity in the range of 5.42-43.36 mg·L-1of pepper alkali concentration (r=0.999 8), and the average recovery of pepper alkali was 100.72% with RSD of 0.56%. Conclusion: The method is simple and accurate, which can be applied to the quality control of the Compound Quchongbanjiuju Pills. |
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| Keywords: | Compound Quchongbanjiuju Pills microscopical identification TLC HPLC pepper alkali |
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