| 黄瑞香茎皮的化学成分研究 |
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| 引用本文： | 廖时余,蒋建勤.黄瑞香茎皮的化学成分研究[J].中草药,2012,43(7):1263-1266. |
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| 作者姓名： | 廖时余 蒋建勤 |
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| 作者单位： | 中国药科大学天然药物化学教研室,江苏南京,211198 |
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| 基金项目： | 国家自然科学基金资助项目(81072537) |
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| 摘 要： | 目的研究黄瑞香Daphne giraldii茎皮的化学成分。方法利用反复硅胶、Sephadex LH-20、ODS以及MCI柱色谱等手段进行分离纯化,并通过NMR、MS等波谱技术进行结构鉴定。结果从黄瑞香茎皮95%乙醇提取物中分离得到7个化合物,分别鉴定为正丁基丁香苷(1)、β-香树脂酮(2)、β-谷甾醇棕榈酸酯(3)、β-香树脂醇乙酸酯(4)、瑞香多林A(5)、狼毒双香豆素(6)、木犀草素(7)。结论化合物1为新化合物,化合物2～4、6为首次从瑞香属植物中分离得到,化合物7为首次从该植物中获得。
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| 关 键 词： | 黄瑞香 瑞香属 正丁基丁香苷 β-香树脂醇乙酸酯 瑞香多林A |
| 收稿时间： | 5/4/2012 12:00:00 AM |
Chemical constituents from stem barks of Daphne giraldii |
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| LIAO Shi-yu and JIANG Jian-qin.Chemical constituents from stem barks of Daphne giraldii[J].Chinese Traditional and Herbal Drugs,2012,43(7):1263-1266. |
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| Authors: | LIAO Shi-yu and JIANG Jian-qin |
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| Institution: | Department of Natural Medicinal Chemistry,China Pharmaceutical University,Nanjing 211198,China |
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| Abstract: | Objective To study the chemical constituents from the stem barks of Daphne giraldii.Methods The components were isolated and purified by chromatography on silica gel,Sephadex LH-20,ODS,and MCI columns,and their structures were identified by NMR and MS.Results Seven compounds were isolated and elucidated as n-butylsyringin(1),β-amyrone(2),β-sitosterol palmitate(3),β-amyrin acetate(4),daphnodorin A(5),bicoumastechamin(6),and luteolin(7).Conclusion Compound 1 is a new compound,compound 7 is firstly obtained from D.giraldii,and compounds 2—4 and 6 are isolated from the plants in Daphne Linn.for the first time. |
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| Keywords: | Daphne giraldii Nitsche Daphne Linn n-butylsyringin β-amyrin acetate daphnodorin A |
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