| 穿龙骨刺胶囊质量标准研究 |
| |
| 引用本文： | 姜明章,冯景辉,孙大勇,李俊平.穿龙骨刺胶囊质量标准研究[J].齐鲁药事,2011,30(3):142-143,145. |
| |
| 作者姓名： | 姜明章 冯景辉 孙大勇 李俊平 |
| |
| 作者单位： | 烟台大洋制药有限公司,山东,烟台,265500 |
| |
| 摘 要： | 目的建立穿龙骨刺胶囊的质量标准控制方法。方法采用薄层色谱法对本品中的穿山龙、枸杞子、淫羊藿进行薄层鉴别;采用高效液相色谱法对本品中的淫羊藿苷进行含量测定。结果在薄层色谱图中可检出穿山龙、枸杞子、淫羊藿;淫羊藿苷在进样量0.2236~4.472μg范围内,与峰面积呈良好的线性关系(r=0.999 9),平均回收率为100.79%(RSD=1.49%)。结论所建立的方法可靠、准确、专属性强,可有效控制穿龙骨刺胶囊的质量。
|
| 关 键 词： | 质量标准 穿龙骨刺胶囊 淫羊藿苷 高效液相色谱法 薄层色谱法 |
Study on the quality standard for Chuanlong Guci Capsules |
| |
| JIANG Ming-zhang,FENG Jing-hui,SUN Da-yong,LI Jun-ping.Study on the quality standard for Chuanlong Guci Capsules[J].qilu pharmaceutical affairs,2011,30(3):142-143,145. |
| |
| Authors: | JIANG Ming-zhang FENG Jing-hui SUN Da-yong LI Jun-ping |
| |
| Institution: | (Yantai Dayang Pharmaceutical Co.,Ltd.,Yantai 265500,China) |
| |
| Abstract: | Objective To establish the quality standard for Chuanlong Guci Capusles.Methods The Dioscorea nipponica,Barbary wolfberry fruit,Epimedium were identified by TLC;The content of icariin was dentermined by HPLC.Results The spots of TLC were quite clear,the linear range of icariin was 0.223 6 μg～4.472 μg（r=0.9999）,the average recovery was 100.79% with RSD 1.49%.Conclusion The method was reliable,specific,accurate,and can effectively control the quality of Chuanlong Guci Capusles. |
| |
| Keywords: | Quality standard Chuanlong Guci Capusles Icariin HPLC TLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
