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| HPLC法测定慢肝解郁胶囊中丹酚酸B的含量 | |
| 引用本文： | 于文静,曾凤英,郭红军.HPLC法测定慢肝解郁胶囊中丹酚酸B的含量[J].中国药事,2012,26(4):382-384. |
| 作者姓名： | 于文静 曾凤英 郭红军 |
| 作者单位： | 1. 吉林省药品检验所,长春,130033 2. 长春医学高等专科学校 3. 吉林省食品药品认证和培训中心 |
| 摘 要： | 目的 建立慢肝解郁胶囊中丹酚酸B的含量测定方法.方法 采用HPLC法.色谱柱:Diamonsil C18;流动相:甲醇乙腈-甲酸-水(30∶10∶1∶59);检测波长:286 nm.结果 丹酚酸B进样量在0.204～3.063 μg范围内线性关系良好.平均加样回收率为98.90％,RSD为0.59％.结论 本法简便、灵敏、准确,可用于慢肝解郁胶囊的质量控制. |
| 关 键 词： | 丹酚酸B 慢肝解郁胶囊 高效液相色谱 |
Determination of Salvianolicacid B in Mangan Jieyu Capsules by HPLC |
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| Yu Wenjing , Zeng Fengying , Guo Hongjun.Determination of Salvianolicacid B in Mangan Jieyu Capsules by HPLC[J].Chinese Pharmaceutical Affairs,2012,26(4):382-384. | |
| Authors: | Yu Wenjing Zeng Fengying Guo Hongjun |
| Institution: | 2(Jilin Institute for Food and Drug Control,Changchun 130033;1Changchun Medicinal College;2Jilin Certification and Training Center for Food and Drug) |
| Abstract: | Objective To develop an assay method for determination of Salvianolicacid B in Mangan Jieyu Capsules by HPLC.Methods The analysis was performed on Diamonsil C18 column.The mobile phase was methanol-acetonitrile-formic acid-water(30∶10∶1∶59).The detection wavelength was at 286 nm.Results The linear range of Salvianolicacid B was 0.204 3～3.063 μg.The average recovery was 98.90%,and RSD was 0.59%.Conclusion The method is simple,rapid and accurate,which is suitable for the quality control of Mangan Jieyu Capsules. |
| Keywords: | Salvianolicacid B Mangan Jieyu Capsules HPLC |
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