| HPLC法测定少腹逐瘀丸中芍药苷的含量 |
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| 引用本文： | 于文静,李井涛. HPLC法测定少腹逐瘀丸中芍药苷的含量[J]. 中国药事, 2012, 26(3): 285-287 |
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| 作者姓名： | 于文静 李井涛 |
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| 作者单位： | 吉林省食品药品检验所,长春,130033 |
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| 摘 要： | 目的 建立HPLC法测定少腹逐瘀丸中芍药苷的含量.方法 色谱柱:Agilent HC C18;乙腈-0.1％磷酸溶液(14∶86)为流动相；检测波长为230nm;柱温为35℃.结果 芍药苷在0.06732～1.3464μg范围内呈良好的线性关系,r=0.9999;平均回收率(n=6)为103.9％,RSD=1.2％.结论 本法简便、准确、重复性好,可作为少腹逐瘀丸的质控方法.
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| 关 键 词： | 少腹逐瘀丸 芍药苷 含量 高效液相色谱 |
Determination of Paeoniflorin in Shaofuzhuyu Pills by HPLC |
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| Yu Wenjing , Li Jingtao. Determination of Paeoniflorin in Shaofuzhuyu Pills by HPLC[J]. Chinese Pharmaceutical Affairs, 2012, 26(3): 285-287 |
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| Authors: | Yu Wenjing Li Jingtao |
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| Affiliation: | Yu Wenjing and Li Jingtao(Jilin Institute for Food and Drug Control,Changchun 130033) |
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| Abstract: | Objective To establish a HPLC method for determination of paeoniflorin in Shaofuzhuyu Pills.Methods A column of Agilent HC C18 was adopted,and the mobile phase was the mixture of acetonitrile-0.1% phosphoric acid(14∶ 86).The detection wavelength was set at 230nm.The column temperature was 35℃.Results Paeoniflorin showed a good linear relationship in the range of 0.06732~1.3464μg(r=0.9999).The average recovery(n=6) was 103.9%(RSD=1.2%).Conclusion The method is simple,accurate and reproducible,which can be used for the quality control of Shaofuzhuyu Pills. |
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| Keywords: | Shaofuzhuyu Pills paeoniflorin determination HPLC |
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