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何首乌商品药材的鉴定与质量分析
引用本文:张勉,徐德然,张紫佳,王峥涛.何首乌商品药材的鉴定与质量分析[J].中国药学杂志,2005,40(11):823-825.
作者姓名:张勉  徐德然  张紫佳  王峥涛
作者单位:中国药科大学生药学研究室,江苏,南京,210038
基金项目:国家中医药管理局科研项目
摘    要: 目的通过对市场药材的鉴定和质量分析,了解何首乌药材的质量状况。方法采用数码显微鉴定、TLC和HPLC的方法对来自全国12个地区的何首乌药材进行了研究。结果12件何首乌商品药材均为正品,根据性状、显微构造和TLC图谱可明显分为2大类型;2,3,5,4’-四羟基二苯乙烯-2-O-β-D-葡萄糖苷含量的结果有力地支持了何首乌2大类型存在的客观性。结论显微图谱对于商品药材的鉴定具有现实意义。何首乌商品药材2大类型的首次发现,对于何首乌质量的评价具有重要的意义。

关 键 词:何首乌  2大类型  性状与显微特征  TLC图谱  高效液相色谱  含量测定
文章编号:1001-2494(2005)11-0823-04
收稿时间:2004-08-15;

Identification and quality analysis on commercial herbs of Radix Polygoni Multiflori
ZHANG Mian,XU De-ran,ZHANG Zi-jia,WANG Zheng-tao.Identification and quality analysis on commercial herbs of Radix Polygoni Multiflori[J].Chinese Pharmaceutical Journal,2005,40(11):823-825.
Authors:ZHANG Mian  XU De-ran  ZHANG Zi-jia  WANG Zheng-tao
Institution:Department of Pharmacognosy, China Pharmaceutical University, Nanjing 210038,China
Abstract:OBJECTIVE To investigate the quality status of Radix Polygoni Multiflori(RPM, Heshouwu) through the identification and analysis of the commercial herbs.METHODS 12 samples collected from different areas in China were studied by the microscopic method, TLC and HPLC. RESULTS Although the samples were all genuine, they were obviously divided into two types according to the macro-and microscopic features and TLC chromatograms. The determination of 2,3,5,4'-tetrahydroxy stilbene-2-O-β-D-glucoside in 12 samples by HPLC supported the two types above. CONCLUSION The digital microscopic pictures provided were actual and used for the identification of the commercial RPM.The discovery of the two types of RPM was significant for its quality evaluation.
Keywords:Radix Polygom Multiflori  two types  macro-and microscopic features  TLC chromatograms  HPLC  determination
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