| 灰毡毛忍冬的指纹图谱研究 |
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| 引用本文： | 陈雨,单宇,贾晓东,刘培,冯煦,梁敬钰.灰毡毛忍冬的指纹图谱研究[J].现代中药研究与实践,2007,21(1):37-40. |
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| 作者姓名： | 陈雨 单宇 贾晓东 刘培 冯煦 梁敬钰 |
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| 作者单位： | 1. 中国药科大学天然药物化学教研室,江苏,南京,210014
2. 江苏省中国科学院植物研究所,南京中山植物园,江苏省药用植物研究开发中心,江苏,南京,210014 |
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| 基金项目： | 江苏省社会发展科技计划BS2001025 |
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| 摘 要： | 目的研究灰毡毛忍冬的指纹图谱。方法高效液相色谱法,二级管阵列检测器(DAD),乙腈-0.4%磷酸溶液(15∶85);流速:1.0 mL/m in;检测波长:327 nm。结果精密度、稳定性、重复性试验中各共有峰相对保留时间和相对峰面积的RSD均<3%,10批样品间具有很高的相似度。结论本方法可以作为山银花药材的质量控制方法。
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| 关 键 词： | 灰毡毛忍冬 山银花 指纹图谱 HPLC |
| 文章编号： | 1004-2199（2007）01-0037-04 |
| 收稿时间： | 2006-11-22 |
| 修稿时间： | 2006年11月22 |
Study on the Fingerprint of Lonicera macranthoides Hand-Mazz |
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| CHEN Yu,SHAN Yu,JIA Xiao-dong,LIU Pei,FENG Xu,LIANG Jing-yu.Study on the Fingerprint of Lonicera macranthoides Hand-Mazz[J].Research and Practice on Chinese Medicines,2007,21(1):37-40. |
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| Authors: | CHEN Yu SHAN Yu JIA Xiao-dong LIU Pei FENG Xu LIANG Jing-yu |
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| Abstract: | Objective To establish HPLC fingerprints of Lonicera macranthoides Hand.-Mazz..Methods HPLC was applied on Agilent Eclipse CDB-C18 column with acetonitrile-0.4% phosphoricacid solution,flow rate of 1.0 mL·min-1.Determination were carried out by PAD and wavelength was at 327 nm.Results RSD of relative retention time and peak area of coexist peaks meet to method requirement during the investigation of precision,stability and repeatability trials.All of the 10 batches of samples shared a high similarity.Conclusion The fingerprint of Lonicera macranthoides Hand.-Mazz.could be used as method for control quality of Shanyinhua. |
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| Keywords: | Lonicera macranthoides Hand -Mazz Shanyinhua fingerprint HPLC |
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