| 益心片的质量标准研究 |
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| 引用本文： | 王凤云,李士明,曾丽云,詹丽玲,张军. 益心片的质量标准研究[J]. 中药材, 2006, 29(3): 286-289 |
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| 作者姓名： | 王凤云 李士明 曾丽云 詹丽玲 张军 |
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| 作者单位： | 广州中医药大学,广东,广州,510405 |
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| 摘 要： | 目的：建立益心片（人参、黄芪、川芎、五味子，丹参等）的质量标准。方法：用TLC法对人参、黄芪、川芎、五味子进行了定性鉴别；用HPLC法测定了益心片中丹酚酸B的含量。结果：定性鉴别分离度好，专属性强；丹酚酸B的含量测定中样品以100倍甲醇为溶媒，超声30min，在C18柱上以乙腈旬．05％磷酸为流动相梯度洗脱，在波长280nm处检测。丹酚酸B在0．12504～2.50080μg范围内线性关系良好，r=0，9999，平均加样回收率为99.35％，RSD为1．02％。结论：方法简便准确、灵敏度高，可用于益心片的质量控制。
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| 关 键 词： | 人参 黄芪甲苷 川芎 五味子 丹酚酸B 质量标准 |
| 文章编号： | 1001-4454(2006)03-0286-04 |
| 收稿时间： | 2005-09-07 |
| 修稿时间： | 2005-09-07 |
Study on Quality Standard of Yixin Tablet |
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| WANG Feng-yun,LI Shi-ming,ZENG Li-yun,Zhan Li-ling,ZHANG Jun. Study on Quality Standard of Yixin Tablet[J]. Journal of Chinese medicinal materials, 2006, 29(3): 286-289 |
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| Authors: | WANG Feng-yun LI Shi-ming ZENG Li-yun Zhan Li-ling ZHANG Jun |
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| Affiliation: | Guangzhou University of Traditional Chinese Medicine, Guangzhou 510405, China |
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| Abstract: | OBJECTIVE:T o determine the quality standard of Yixin Tablet. METHODS: The nature differentiation of Radix Ginseng, Radix Astragali, Rhizoma Chuanxiong, Fructus Schisandrae was determined by TLC and content of salvianolic acid B in Yixin Tablet was determined by HPLC. RESULTS: The nature differentiation separate degree is kind and special attribute was strong. The compounds were base-isolated on the column of C18 which gradient eluted with acetonitrile and H2O (0.05% H3PO4) and detective wavelength was 280 nm. The linearity was obtained over the range of 0.12504-2.50080 microg (r = 0.9999) and the average recovery rate was 99.35%. CONCLUSION: The method is simple, convenient and accurate. The sensitivity is high. It can be used in the quality control of Yixin Tablet. |
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