| 高效液相色谱法测定板草抗病毒颗粒中牛蒡苷的含量 |
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| 引用本文： | 汤迎爽,宋红儒,康阿龙. 高效液相色谱法测定板草抗病毒颗粒中牛蒡苷的含量[J]. 解放军药学学报, 2011, 27(1): 55-56. DOI: 10.3969/j.issn.1008-9926.2011.01.017 |
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| 作者姓名： | 汤迎爽 宋红儒 康阿龙 |
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| 作者单位： | 1. 解放军323医院,陕西西安,710054
2. 解放军451医院,陕西西安,710054 |
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| 摘 要： | 目的 建立测定板草抗病毒颗粒中牛蒡苷的高效液相色谱法.方法 采用色谱柱Kromasi C18色谱柱(4.6mmx250 mm,5μm);流动相为乙腈--水(25:75),检测波长为280 nm.结果 牛蒡苷回归方程为Y=58423.166X+25336.723,在0.408～2.04μg范围内与峰面积具有良好的线性关系...
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| 关 键 词： | 板草抗病毒颗粒 牛蒡苷 高效液相色谱法 |
Determination of Paeoniflorin in Bancao Kangbingdu Granule by High Performance Liquid Chromatography |
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| TANG Ying-shuang,SONG Hong-ru,KANG A-long. Determination of Paeoniflorin in Bancao Kangbingdu Granule by High Performance Liquid Chromatography[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2011, 27(1): 55-56. DOI: 10.3969/j.issn.1008-9926.2011.01.017 |
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| Authors: | TANG Ying-shuang SONG Hong-ru KANG A-long |
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| Affiliation: | ②①Hospital 323 of PLA,Xi＇an 710054,China;②Hospital 451 of PLA,Xi＇an 710054,China |
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| Abstract: | Objective To establish an high performance liquid chromatography method for quantitative determination of Paeoniflorin in Bancao Kangbingdu Granule.Methods The separation was performed on Ultrasphere C18 column（4.6 mm×250 mm,5 μm） with a mobile phase of acetonitrile and water（25∶75）.The UV detection wavelength was 280 nm.Results The linear range of salvianolic acid B was 0.408-2.04 μg,r=0.9999.The mean recovery was 98.0% with RSD was 1.2%（n=6）.Conclusion This method is simple,accurate,sensitive and with good reproducibility. |
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| Keywords: | Bancao Kangbingdu Granule paeoniflorin high performance liquid chromatography |
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