| 橙黄瑞香中苯丙素类成分研究 |
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| 引用本文： | 黄圣卓,王琪,刘玉清,周俊,戴好富,马青云,孔凡栋,赵友兴.橙黄瑞香中苯丙素类成分研究[J].中草药,2016,47(22):3970-3974. |
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| 作者姓名： | 黄圣卓 王琪 刘玉清 周俊 戴好富 马青云 孔凡栋 赵友兴 |
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| 作者单位： | 中国热带农业科学院热带生物技术研究所, 海南 海口 571101;中国热带农业科学院热带生物技术研究所, 海南 海口 571101;中国科学院昆明植物研究所 植物化学与西部资源持续利用国家重点实验室, 云南 昆明 650201;中国科学院昆明植物研究所 植物化学与西部资源持续利用国家重点实验室, 云南 昆明 650201;中国热带农业科学院热带生物技术研究所, 海南 海口 571101;中国热带农业科学院热带生物技术研究所, 海南 海口 571101;中国热带农业科学院热带生物技术研究所, 海南 海口 571101;中国热带农业科学院热带生物技术研究所, 海南 海口 571101 |
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| 基金项目： | 国家自然科学基金青年基金（31300294） |
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| 摘 要： | 目的研究橙黄瑞香Daphne aurantiaca茎的苯丙素类化学成分。方法采用正相和反相硅胶柱色谱与Sephadex LH-20凝胶柱色谱进行分离纯化,并运用波谱方法鉴定化合物的结构。结果从橙黄瑞香茎95%乙醇提取物中分离得到13个苯丙素类成分,分别鉴定为咖啡酸二十三烷酯(1)、咖啡酸二十烷酯(2)、咖啡酸十九烷酯(3)、咖啡酸十八烷酯(4)、咖啡酸十七烷酯(5)、咖啡酸十六烷酯(6)、咖啡酸十四烷酯(7)、咖啡酸十二烷酯(8)、咖啡酸十一烷酯(9)、咖啡酸异戊酯(10)、阿魏酸(11)、3,4-二甲氧基桂皮醛(12)、咖啡醇(13)。结论所有化合物均为首次从该植物中分离得到。
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| 关 键 词： | 瑞香属 橙黄瑞香 苯丙素 咖啡酸酯 阿魏酸 3, 4-二甲氧基桂皮醛 咖啡醇 |
| 收稿时间： | 6/3/2016 12:00:00 AM |
Phenylpropanoids from Daphne aurantiaca |
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| HUANG Sheng-zhuo,WANG Qi,LIU Yu-qing,ZHOU Jun,DAI Hao-fu,MA Qing-yun,KONG Fan-dong and ZHAO You-xing.Phenylpropanoids from Daphne aurantiaca[J].Chinese Traditional and Herbal Drugs,2016,47(22):3970-3974. |
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| Authors: | HUANG Sheng-zhuo WANG Qi LIU Yu-qing ZHOU Jun DAI Hao-fu MA Qing-yun KONG Fan-dong and ZHAO You-xing |
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| Institution: | Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China;Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650201, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650201, China;Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China;Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China;Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China;Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agriculture Sciences, Haikou 571101, China |
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| Abstract: | Objective To study the phenylpropanoids from Daphne aurantiaca. Methods The constituents were separated by column chromatography, their structures were elucidated by spectral data analyses. Results Thirteen phenylpropanoids were isolated from the EtOAc extract and were identified as caffeic acid tricosyl ester (1), caffeic acid eicosanyl ester (2), caffeic acid nonadecyl ester (3), caffeic acid octadecyl ester (4), caffeic acid heptadecyl ester (5), caffeic acid hexadecyl ester (6), caffeic acid tetradecyl ester (7), caffeic acid dodecyl ester (8), caffeic acid undecyl ester (9), caffeic acid isopentyl ester (10), ferulic acid (11), 3,4-dimethoxy-cinnamaldehyde (12), and caffeic alcohol (13). Conclusion The compounds are obtained from this plant for the first time. |
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| Keywords: | Daphne Linn Daphne aurantiaca Diels phenylpropanoid caffeic acid ester ferulic acid 3, 4-dimethoxy-cinnamaldehyde caffeic alcohol |
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