| 青蒿素抗心律作用研究 |
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| 引用本文： | 杜智敏,刘影. 青蒿素抗心律作用研究[J]. 中国药学杂志, 2003, 38(5): 372-372 |
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| 作者姓名： | 杜智敏 刘影 |
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| 作者单位： | 1. 哈尔滨医科大学附属二院临床药理学研究所,黑龙江,哈尔滨,150086
2. 哈尔滨医科大学药理教研室,黑龙江,哈尔滨,150086 |
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| 摘 要： | 目的研究前列泌尿栓质量控制方法，制定其质量标准。方法采用薄层色谱法对前列泌尿栓2种药物进行定性鉴别，采用高效液相色谱法测定黄柏中盐酸小檗碱和血竭中血竭素的含量。结果2种药物薄层定性鉴别重现性好，斑点圆整；盐酸小檗碱和血竭素平均回收率分别为98.83%(RSD为1.69%)和98.17%(RSD为1.06%)。结论本方法专属性强，结果准确，检验快速，可有效控制前列泌尿栓的质量。
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| 关 键 词： | 前列泌尿栓 高效液相色谱法 小檗碱 |
| 文章编号： | 1001-2494(2003)05-0372-01 |
| 收稿时间： | 2001-11-15; |
| 修稿时间： | 2002-09-30 |
The study on artemisinin antiarrhythmic action |
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| ZHANG Cui-ying,LI Zhen-guo,LEI Liu-cheng. The study on artemisinin antiarrhythmic action[J]. Chinese Pharmaceutical Journal, 2003, 38(5): 372-372 |
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| Authors: | ZHANG Cui-ying LI Zhen-guo LEI Liu-cheng |
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| Affiliation: | Henan Institute of Drug Control,Zhengzhou 450003,China |
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| Abstract: | OBJECTIVE To establish a specific assay for Qianlie Miniao suppository.METHOD TLC was used to make a qualitative determination for 2 drugs in the formulary.The contents of berberine and dracorhobin were determined by HPLC.RESULTS 2 drugs in the formulary were identified with good repetition.The average recovery of berberine and dracorhobin were 98.83%(RSD 1.69%) and 98.17%(RSD 1.06%)respectively.CONCLUSION The method was sensitive,accurate and rapid.It was helpful to establish specification for Qianlie Miniao suppository. |
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| Keywords: | Qianlie Miniao suppository HPLC dracorhobin berberine |
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