| 血浆中盐酸氟桂嗪的荧光分光光度测定法 |
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| 引用本文： | 郭琦,刘海静,明新,张阿慧,杨云,陈慧娟.血浆中盐酸氟桂嗪的荧光分光光度测定法[J].中国现代应用药学,1997,14(5):9-11. |
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| 作者姓名： | 郭琦 刘海静 明新 张阿慧 杨云 陈慧娟 |
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| 作者单位： | 西安医科大学药学院!西安，710061，陕西省药品检验所，西安医科大学药学院!西安，710061，西安医科大学药学院!西安，710061，西安医科大学药学院!西安，710061，西安医科大学药学院!西安，710061 |
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| 摘 要： | 建立了血浆样品中盐酸氟桂的荧光分光光度测定法，血浆样品经碱化用正己烷提取，水浴挥干正己烷后，用０．１ｍｏｌ／ＬＨＣｌ定容，在激发波长２６０ｎｍ，发射波长３１０ｎｍ处测定荧光强度，最低检出浓度１０ｎｇ／ｍｌ。线性范围２．０－３０．０μｇ／ｍｌ（ｒ＝０．９９０７），平均回收率为１００．０８％，ＲＳＤ为５．０３％（ｎ＝９），日内，日间精密度分别为１．６３％～３．２８％和１．９４％～５．９５％。方法简便，
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| 关 键 词： | 盐酸氟桂嗪 血药浓度 荧光分光光度法 |
Determination of Flunarizine Hydrochloride in Human Plasma by Fluorometry |
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| GuoQi;LiuHaijin;MingXin;ZhangAhui;YangYun;ChenHuijuan..Determination of Flunarizine Hydrochloride in Human Plasma by Fluorometry[J].The Chinese Journal of Modern Applied Pharmacy,1997,14(5):9-11. |
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| Authors: | GuoQi;LiuHaijin;MingXin;ZhangAhui;YangYun;ChenHuijuan |
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| Institution: | College of Pharmacy Xi'an Medical University Xi'an710061 |
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| Abstract: | A fluorometric method was established for the determination of flunarizine hydrochloride in human plasma. The drug was extracted from akalized plasma into nhexane. Oxganic extractant was dried under bath water.The residue was dissolved in 0.1mol/LHCl. Flu |
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| Keywords: | flunarizine hydrochloride fluorometry plasma concentration |
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