| 野独活茎化学成分的分离与鉴定 |
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| 引用本文： | 雷 雨,吴立军,毕 丹,孙精伟,屠鹏飞. 野独活茎化学成分的分离与鉴定[J]. 沈阳药科大学学报, 2009, 26(2): 104-107 |
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| 作者姓名： | 雷 雨 吴立军 毕 丹 孙精伟 屠鹏飞 |
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| 作者单位： | 雷雨,吴立军,LEI Yu,WU Li-jun(沈阳药科大学,中药学院,辽宁,沈阳,110016);毕丹,孙精伟,屠鹏飞,BI Dan,SUN Jing-wei,TU Peng-fei(北京大学,药学院,北京,100083) |
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| 基金项目： | 教育部长江学者创新团队基金 |
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| 摘 要： | 目的更好地开发利用野独活(Miliusa balansae Fin. et Gag.)药用植物资源。方法用质量分数为80%的乙醇提取,用硅胶柱色谱、羟丙基葡聚糖凝胶LH-20柱色谱分离纯化;通过NMR谱和薄层色谱等鉴定化合物的结构。结果分离鉴定了10个化合物,分别为尿囊素(allantion,1)、(+)-衡州乌药碱(coclaurine,2)、1-N-甲基乌药碱(1-N-methylcoclaurine,3)、鹅掌揪碱(liriodenine,4)、腺嘌呤核苷(adenine riboside,5)、尿嘧啶核苷(uridine,6)、蔗糖(sucrose,7)、葡萄糖(glucose,8)、β-谷甾醇(β-sitosterol,9)、胡萝卜苷(daucosterol,10)。结论除化合物4外,其他化合物均为首次从野独活属植物中分离得到。
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| 关 键 词： | 野独活 化学成分 结构鉴定 生物碱 |
| 收稿时间： | 2008-04-08 |
Isolation and identification of chemical constituents from stems of Miliusa balansae Fin. et Gag. |
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| LEI Yu,WU Li-jun,BI Dan,SUN Jing-wei,TU Peng-fei. Isolation and identification of chemical constituents from stems of Miliusa balansae Fin. et Gag.[J]. Journal of Shenyang Pharmaceutical University, 2009, 26(2): 104-107 |
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| Authors: | LEI Yu WU Li-jun BI Dan SUN Jing-wei TU Peng-fei |
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| Affiliation: | (1. School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang 110016, China; 2. School of Pharmacy, Peking University , Beijing 100083, China ) |
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| Abstract: | Abstract: Objective To study the chemical constituents of stems of Miliusa balansae Fin. et Gag. Methods The compounds were isolated by various column chromatographic methods; and their structures were identified by TLC and spectra analysis. Results Ten compounds were obtained and identified as allantion（1）,coclaurine（2）,1-N-methylcoclaurine（3）,liriodenine （4）, adenine riboside（5）,uridine（6）,sucrose（7）, glucose（8）,β-sitosterol（9）and daucosterol（10）,respectively. Conclusions The nine compounds are obtained from this genus for the first time except for the compound 4. |
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| Keywords: | Miliusa balansae Fin. et Gag. chemical constituent structure identification ')" >alkaloid |
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