| HPLC法测定银杏内酯滴丸中银杏内酯A及银杏内酯B总量 |
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| 引用本文： | 吴 云,颜丙鹏,毕宇安,仲 艳,萧 伟.HPLC法测定银杏内酯滴丸中银杏内酯A及银杏内酯B总量[J].世界科学技术-中医药现代化,2012,14(2):1498-1501. |
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| 作者姓名： | 吴 云 颜丙鹏 毕宇安 仲 艳 萧 伟 |
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| 作者单位： | 江苏康缘药业股份有限公司/中药制药过程新技术国家重点实验室 连云港 222001 |
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| 基金项目： | 科学技术部国家重大新药创制项目（2011ZX09401-097）：中药治疗心脑血管疾病有效成份组（群）的创新药物孵化基地，负责人：萧伟。 |
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| 摘 要： | 目的:建立银杏内酯滴丸中银杏内酯A、银杏内酯B含量测定方法。方法:采用高效液相色谱法,以正丙醇-四氢呋喃-水(1∶27∶72)为流动相,流速:1.0 mL.min-1,检测波长:220 nm。结果:建立了银杏内酯滴丸中银杏内酯A、银杏内酯B含量测定方法,且银杏内酯A、银杏内酯B的RSD分别为1.39%,2.16%。结论:本方法简便可靠,可用于银杏内酯滴丸的质量控制。
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| 关 键 词： | 银杏内酯滴丸 银杏内酯A 银杏内酯B |
| 收稿时间： | 1/8/2011 12:00:00 AM |
| 修稿时间： | 2011/1/28 0:00:00 |
HPLC Determination of Ginkgolide A and Ginkgolide B Content in Ginkgolide Dropping Pills |
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| Wu Yun,Yan Bingpeng,Bi Yu''an,Zhong Yan and Xiao Wei.HPLC Determination of Ginkgolide A and Ginkgolide B Content in Ginkgolide Dropping Pills[J].World Science and Technology-Modernization of Traditional Chinese Medicine,2012,14(2):1498-1501. |
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| Authors: | Wu Yun Yan Bingpeng Bi Yu'an Zhong Yan and Xiao Wei |
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| Institution: | Jiangsu Kanion Pharmaceutical Co., Ltd., Lianyungang 222001, China; State Key Laboratory of New-tech for Chinese Medicine Pharmaceutical Process, Lianyungang 222001, China |
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| Abstract: | This study was aimed to establish the method of determining ginkgolide A and ginkgolide B content in ginkgolide dropping pills.High performance liquid chromatography(HPLC) was used in the research with N-propanol-THF-water(1∶27∶72) as the mobile phase.The flow rate was 1 mL·min-1.And the detection wavelength was at 220 nm.The results showed that the determination method of ginkgolide A and ginkgolide B content in ginkgolide dropping pills was established.And the RSD of ginkgolide A and ginkgolide B were 1.39% and 2.16%,respectively.It was concluded that this method is simple and reliable,which can be used for quality control of ginkgolides dropping pills. |
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| Keywords: | Ginkgolide dropping pills ginkgolide A ginkgolide B |
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