| 高效液相色谱法测定蛭芎活血丸中阿魏酸的含量 |
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| 引用本文： | 邓松岳.高效液相色谱法测定蛭芎活血丸中阿魏酸的含量[J].中国中医药咨讯,2011,3(6):310-311. |
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| 作者姓名： | 邓松岳 |
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| 作者单位： | 商丘市食品药品检验所,河南,商丘,476000 |
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| 摘 要： | 目的建立HPLC法测定蛭芎活血丸中阿魏酸含量的方法。方法采用EclipseXDB-C18色谱柱，甲醇-1％醋酸溶液（22：78）为流动相；流速1．0ml？min-1；检测波长322nm。结果阿魏酸在6．258～31．29μg？ml-1范围内线性关系良好（r=-0．9998），平均回收率为98．65％，RSD=1．2l％（n=6）。结论本方法操作简便，专属性强，结果准确，可用于蛭芎活血丸的质量控制。
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| 关 键 词： | 高效液相色谱法 阿魏酸 含量测定 |
Determination of ferulic acid in zhixionghuoxue pills by HPLC |
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| Deng Songyue.Determination of ferulic acid in zhixionghuoxue pills by HPLC[J].Journal of China Traditional Chinese Medicine Information,2011,3(6):310-311. |
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| Authors: | Deng Songyue |
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| Institution: | Deng Songyue(Shangqiu Institute for Food and Drug Control,Shangqiu, Henan 476000) |
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| Abstract: | Objective： To establish a HPLC method to determinate ferulic acid in zhixionghuoxue pills. Method： The chromatographic system consisted of C18 column,using Methanol-1% Acetic acid glacial （22：78） as mobile phase.The content was detected at a waveleng of 322nm,the flow rate was 1.0ml.min-1 .Results： The curcumin have a good tincar rolatim in the range of 6.258-31.29μ g. ml-1（r=-0.9998）,the average recovery was 98.65% and RSD=1.21%（n=6）. Conolusion： The established method is accuracy ,sensitive and simple.It can be used for quality control of zhixionghuoxne pills. |
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| Keywords: | HPLC Ferulic acid Determination |
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