| 黄芩配伍知母后黄芩中主要黄酮类成分的含量变化 |
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| 引用本文： | 史芳,李清,陈晓辉,刘莉,张天虹,毕开顺.黄芩配伍知母后黄芩中主要黄酮类成分的含量变化[J].中国实验方剂学杂志,2011,17(17):84-87. |
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| 作者姓名： | 史芳 李清 陈晓辉 刘莉 张天虹 毕开顺 |
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| 作者单位： | 沈阳药科大学药学院,沈阳,110016 |
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| 摘 要： | 目的:考察黄芩与知母配伍后黄芩中主要黄酮类成分含量的变化。方法:采用反相高效液相色谱法,Kromasil C18色谱柱(4.6 mm×250 mm5,.0μm),流动相甲醇-乙腈-0.2%磷酸溶液梯度洗脱,流速1 mL.min-1,检测波长276 nm,柱温30℃。结果:黄芩苷、汉黄芩苷、黄芩素和汉黄芩素分别在9.76～195.2(r=0.999 2),3.960～79.20(r=0.999 9),1.600～32.00(r=0.999 5),1.536～30.72 mg.L-1(r=0.999 9)与峰面积线性关系良好;平均加样回收率(n=9)均在96.8%～103.0%,RSD均小于1.7%。结论:黄芩与知母配伍后使黄芩水煎液中的4种黄酮类成分含量显著增加。
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| 关 键 词： | 黄芩 知母 药对 配伍 高效液相色谱法 |
| 收稿时间： | 2011/3/17 0:00:00 |
Influence on Main Flavone Ingredients in Scutellaria after Compatibility with Rhizome Anemarrhenae |
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| SHI Fang,LI Qing,CHEN Xiao-hui,LIU Li,ZHANG Tian-hong and BI Kai-shun.Influence on Main Flavone Ingredients in Scutellaria after Compatibility with Rhizome Anemarrhenae[J].China Journal of Experimental Traditional Medical Formulae,2011,17(17):84-87. |
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| Authors: | SHI Fang LI Qing CHEN Xiao-hui LIU Li ZHANG Tian-hong and BI Kai-shun |
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| Institution: | School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China;School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China;School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China;School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China;School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China;School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China |
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| Abstract: | |
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| Keywords: | Radix Scutellariae Rhizoma Anemarrhenae couple of traditional chinese medicine compatibility HPLC |
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