| 吴茱萸苦味拆分组分物质基础研究 |
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| 引用本文： | 杨志欣,孟永海,王秋红,杨炳友,匡海学. 吴茱萸苦味拆分组分物质基础研究[J]. 中国实验方剂学杂志, 2011, 17(21): 74-77 |
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| 作者姓名： | 杨志欣 孟永海 王秋红 杨炳友 匡海学 |
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| 作者单位： | 黑龙江中医药大学北药基础与应用研究省部共建教育部重点实验室、黑龙江省中药及天然药物药效物质基础研究重点实验室,哈尔滨,150040 |
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| 基金项目： | 国家重点基础研究发展(973)计划项目(2006CB504708) |
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| 摘 要： | 目的:研究疏毛吴茱萸苦味拆分组分——95%乙醇洗脱组分的物质基础。方法:采用硅胶柱色谱、ODS反相柱色谱以及HPLC等现代分离技术与方法进行分离纯化,根据化合物的理化性质和波谱学数据进行结构鉴定。结果:从疏毛吴茱萸苦味拆分组分———95%乙醇洗脱组分中分离并鉴定了7个化合物,分别为水仙苷(narcissin)(Ⅰ)、异鼠李素-3-O-半乳糖苷(isorhamnetin-3-O-galactoside)(Ⅱ)、金丝桃苷(hyperoside)(Ⅲ)、异槲皮苷(isoquercitrin)(Ⅳ)、紫丁香苷(syringoside)(Ⅴ)、β-谷甾醇(Ⅵ)、去氢柠檬苦素(dehydrolimonin)(Ⅶ)。结论:吴茱萸苦味拆分组分———95%乙醇洗脱组分的物质基础有黄酮、柠檬苦素类等成分。化合物Ⅰ,Ⅳ,Ⅴ为首次从该植物中分离得到。
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| 关 键 词： | 疏毛吴茱萸 物质基础 化学成分 性味 苦味 |
| 收稿时间： | 2011-06-22 |
Substance Basis of Bitter Resolution and Composition from Fructus Evodiae |
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| YANG Zhi-xin,MENG Yong-hai,WANG Qiu-hong,YANG Bing-you and KUANG Hai-xue. Substance Basis of Bitter Resolution and Composition from Fructus Evodiae[J]. China Journal of Experimental Traditional Medical Formulae, 2011, 17(21): 74-77 |
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| Authors: | YANG Zhi-xin MENG Yong-hai WANG Qiu-hong YANG Bing-you KUANG Hai-xue |
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| Affiliation: | Key Laboratory of Chinese Materia Medica(Heilongjiang University of Chinese Medicine), Ministry of Education, Heilongjang Key Laboratory of TCM Pharmacodynamic Material Bases, Harbin 150040, China;Key Laboratory of Chinese Materia Medica(Heilongjiang University of Chinese Medicine), Ministry of Education, Heilongjang Key Laboratory of TCM Pharmacodynamic Material Bases, Harbin 150040, China;Key Laboratory of Chinese Materia Medica(Heilongjiang University of Chinese Medicine), Ministry of Education, Heilongjang Key Laboratory of TCM Pharmacodynamic Material Bases, Harbin 150040, China;Key Laboratory of Chinese Materia Medica(Heilongjiang University of Chinese Medicine), Ministry of Education, Heilongjang Key Laboratory of TCM Pharmacodynamic Material Bases, Harbin 150040, China;Key Laboratory of Chinese Materia Medica(Heilongjiang University of Chinese Medicine), Ministry of Education, Heilongjang Key Laboratory of TCM Pharmacodynamic Material Bases, Harbin 150040, China |
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| Abstract: | |
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| Keywords: | Evodia rutaecarpa (Juss.) Benth. Var. bodinieri (Dode) Huang substance basis chemical constituents character and taste bitter |
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