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| 小叶丁香苷类化学成分研究 | |
| 引用本文： | 刘普,杨友亮,邓瑞雪,赵天增,尹卫平. 小叶丁香苷类化学成分研究[J]. 中国实验方剂学杂志, 2011, 17(19): 127-131 |
| 作者姓名： | 刘普 杨友亮 邓瑞雪 赵天增 尹卫平 |
| 作者单位： | 1. 河南科技大学化工与制药学院,河南洛阳471003;河南省科学院天然产物重点实验室,郑州 450002 2. 河南科技大学化工与制药学院,河南洛阳,471003 3. 河南省科学院天然产物重点实验室,郑州,450002 |
| 基金项目： | 河南科技大学博士科研启动基金(09001244) |
| 摘 要： | 目的:研究药用植物小叶丁香的苷类化学成分。方法:采用硅胶柱色谱,Toyopearl HW-40C,Sephadex LH-20等多种柱色谱分离,制备高效液相色谱对有效部位进行分离、纯化,根据波谱数据分析鉴定化合物结构。结果:从小叶丁香的乙酸乙酯和正丁醇层分离得到8个糖苷类化合物,分别鉴定为橄榄苦苷(oleuropein,1),(8Z)-ligstroside(2),10-hrdroxyoleosidedimethyl ester(3),grandifloroside(4),松果菊苷(echinacoside,5),类叶升麻苷(verbascoside,6),异类叶升麻苷(isoverbascoside,7),连翘酯苷B(forsythoside B,8)。结论:化合物2～8为首次从中小叶丁香中分离得到的化合物,其中化合物3～4为首次从丁香属中分离得到的化合物。 |
| 关 键 词： | 小叶丁香 化学成分 糖苷类化合物 |
| 收稿时间： | 2011-03-26 |
Studies on Chemical Constituents of Glycosides from Syringa pubenscens |
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| LIU Pu,YANG You-liang,DENG Rui-xue,ZHAO Tian-zeng,YIN Wei-ping. Studies on Chemical Constituents of Glycosides from Syringa pubenscens[J]. China Journal of Experimental Traditional Medical Formulae, 2011, 17(19): 127-131 | |
| Authors: | LIU Pu YANG You-liang DENG Rui-xue ZHAO Tian-zeng YIN Wei-ping |
| Affiliation: | LIU Pu1,2,YANG You-liang1,DENG Rui-xue1,ZHAO Tian-zeng2,YIN Wei-ping1(1.Chemical Engineering & Pharmaceutical College,Henan University of Science and Technology,Luoyang 471003,China,2.Key Laboratory of Natural Products,Henan Academy of Sciences,Zhengzhou 450002,China) |
| Abstract: | Objective:To study the chemical constituents of Syringa pubenscens.Method: Chemical constituents were isolated by Toyopearl HW-40,preparative HPLC,and silica gel column chromatography.The structures were elucidated on the basis of spectral data analysis.Result: Eight compounds,oleuropein(1),(8Z)-ligstroside(2),10-hrdroxyoleoside dimethyl ester(3),grandifloroside(4),echinacoside(5),verbascoside(6),isoverbascoside(7),forsythoside B(8)were isolated from S.pubenscens.Conclusion:Compounds 2-8 were isolated from ... |
| Keywords: | Syringa pubenscens chemical constituents glycoside |
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