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火焰原子吸收光谱法测定鸡内金中的金属元素
引用本文:胡烜红,胡久宏,周炳,胡久梅.火焰原子吸收光谱法测定鸡内金中的金属元素[J].中国实验方剂学杂志,2011,17(21):104-106.
作者姓名:胡烜红  胡久宏  周炳  胡久梅
作者单位:1. 西南交通大学生命科学与工程学院,成都,610031
2. 汶川县林业医院,四川汶川,623000
摘    要:目的:利用原子吸收光谱法测定鸡内金中金属元素含量。方法:使用HNO3-HClO4体系消解样品,采用火焰原子吸收光谱法对鸡内金中的Mg,Fe,Mn,Zn,Cu 5种金属元素进行测定。结果:鸡内金样品中含有较丰富的Mg,Fe,Mn,Zn,Cu。5种金属元素回收率在95.27%~104.47%,RSD<3.53%。结论:建立了鸡内金药材中金属元素的分析方法,该方法操作简便,精密度好,结果准确可靠。

关 键 词:鸡内金  金属元素  火焰原子吸收光谱法
收稿时间:2011/6/10 0:00:00

Determination of Metal Elements in Galli Gigeriae Endotheliun Corneum by Flame Atomic Absorption Spectrometry
HU Xuan-hong,HU Jiu-hong,ZHOU Bing and HU Jiu-mei.Determination of Metal Elements in Galli Gigeriae Endotheliun Corneum by Flame Atomic Absorption Spectrometry[J].China Journal of Experimental Traditional Medical Formulae,2011,17(21):104-106.
Authors:HU Xuan-hong  HU Jiu-hong  ZHOU Bing and HU Jiu-mei
Institution:School of Life Science and Engineering, Southwest Jiaotong University, Chengdu 610031, China;Forest Hospital, Wenchuan 623000, China;School of Life Science and Engineering, Southwest Jiaotong University, Chengdu 610031, China;School of Life Science and Engineering, Southwest Jiaotong University, Chengdu 610031, China
Abstract:Objective: To determine metal elements in Galli Gigeriae Endotheliun Corneum by FAAS. Method: The samples were digested with mixed acid of nitric acid-perchlorate. Mg, Cu, Zn, Fe and Mn in Galli Gigeriae Endotheliun Corneum were determined by flame atomic absorption spectroscopy. Result: Galli Gigeriae Endotheliun Corneum was rich in Mg, Fe, Mn, Zn and Cu;recovery rate was 95.27%-104.47% and the relative standard deviation was 3.53% for each element. Conclusion: The detection method of metal elements of the Galli Gigeriae Endotheliun Corneum is established. The method is rapid, accurate and reliable.
Keywords:Galli Gigeriae Endotheliun Corneum  metal elements  flame atomic absorption spectrometry (FAAS)
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