| 固相微萃取/气相色谱/质谱法分析蔓荆子挥发性化学成分 |
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| 引用本文： | 杨再波,赵超. 固相微萃取/气相色谱/质谱法分析蔓荆子挥发性化学成分[J]. 河南大学学报(医学版), 2006, 25(4): 16-19 |
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| 作者姓名： | 杨再波 赵超 |
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| 作者单位： | 黔南民族师范学院,化学与化工系,贵州,都匀,558000;贵州师范大学,天然药物质量控制研究中心,贵州,贵阳,550001 |
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| 摘 要： | 目的:对蔓荆子挥发油的化学成分进行了分析。方法:采用固相微萃取/气相色谱/质谱(SPME/GC/MS)联用技术。结果:分离出81个组分,确认了其中64种组分,并用归一化法测定其相对百分含量,其相对含量占总挥发性组分峰面积的96.85%。结论:主要成分为:α-蒎烯(4.26%)、1,8-桉树脑5.90(%)、芳樟醇(3.59%)、莰烯(4.89%)、丁子香酚(2.18%)、β-石竹烯(14.72%)、β-古芸烯(2.56%)、双环吉马烯(4.35%)、α-雪松醇(11.29%)。
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| 关 键 词： | 固相微萃取 气相色谱/质谱 蔓荆子 挥发油 |
| 文章编号： | 1672-7606(2006)04-0016-04 |
| 收稿时间： | 2006-10-17 |
| 修稿时间： | 2006-10-17 |
Analysis of chemical constituents of the essential oil from Vitex trifolia L.var.simplicifolia Cham.by SPME-GC-MS |
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| Yang Zai-bo,Zhao Chao. Analysis of chemical constituents of the essential oil from Vitex trifolia L.var.simplicifolia Cham.by SPME-GC-MS[J]. Journal of Henan University, 2006, 25(4): 16-19 |
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| Authors: | Yang Zai-bo Zhao Chao |
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| Affiliation: | 1. Chemistry and Chemical lndustry Department, Qinnan Normal Univesity of Nationalities, Guizhou Duyun 558000, China; 2. Research Center of the Quality Control of Natural medicines of Guizhou Normal University, Guiyang 550001, China |
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| Abstract: | Objective: The chemical components of the essential oil from the Vitex trifolia L.var.simplicifolia Cham.Methods: The chemical components of the essential oil were analyzed by SPME-GC-MS.Results: The total essential oil were separated 81 components, the amount of the components from the essential oil were determined by normalization method,the components separated were identified by GC-MS.Conclusion: There are 64 components which were identified its,α-pinene(4.26%),1,8-cineole(5.90%),Linalol(3.59%),Camphene(4.89%),eugenol(2.18%),beta-Caryophyllene(14.72%),Bicyclogermacrene(4.35),beta.-gurjune(2.56%),alpha.-Cedrol(11.29%),ect.and these components are composed of about 96.85% of the total essential constituents. |
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| Keywords: | SPME GC/MS Vitex trifolia L.var.simplicifolia Cham essential oil |
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