| 通络袪痹丸的质量标准 |
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| 引用本文： | 蒋云根,陈长生,宋彦蓉,付龙根,谢文,徐哲.通络袪痹丸的质量标准[J].第四军医大学学报,2005,26(3):235-237. |
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| 作者姓名： | 蒋云根 陈长生 宋彦蓉 付龙根 谢文 徐哲 |
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| 作者单位： | 武警江西总队医院药剂科,江西,南昌,330001;第四军医大学预防医学系卫生统计学教研室,陕西,西安,710033 |
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| 摘 要： | 目的：建立通络祛痹丸的质量标准．方法：采用薄层色谱法对制剂中的制川乌、三七、当归进行定性鉴别，用二阶导数光谱法测定制剂中乌头碱的含量，结果：3种供试品薄层色谱在与相应对照品或对照药材色谱相应的位置上分别显相同颜色的斑点，含量测定中，乌头碱在0.04～0.26g／L范围内线性关系良好，r=0．9994，平均回收率为99．4％，RSD=1.20％．结论：该方法可用于通络祛痹丸的质量控制。
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| 关 键 词： | 通络袪痹丸 制川乌 三七 当归 乌头碱 薄层色谱 二阶导数光谱 |
| 文章编号： | 1000-2790(2005)03-0235-03 |
| 修稿时间： | 2004年9月28日 |
Quality standard of Tongluo Quebi Pill |
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| JIANG Yun-Gen ,CHEN Chang-Sheng ,SONG Yan-Rong ,FU Long-Gen ,XIE Wen ,XU Zhe.Quality standard of Tongluo Quebi Pill[J].Journal of the Fourth Military Medical University,2005,26(3):235-237. |
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| Authors: | JIANG Yun-Gen CHEN Chang-Sheng SONG Yan-Rong FU Long-Gen XIE Wen XU Zhe |
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| Institution: | JIANG Yun-Gen 1,CHEN Chang-Sheng 2,SONG Yan-Rong 1,FU Long-Gen 1,XIE Wen 1,XU Zhe 1 1Department of Pharmacy,Jiangxi Hospital,Jiangxi Corps of Chinese Armed Police Force,Nanchang 330001,China,2Department of Health Statistics,School of Preventive Medicine,Fourth Military Medical University,Xi'an 710033,China |
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| Abstract: | AIM: To establish a quality standard of Tongluo Quebi Pill (TQP). METHODS: Thin layer chromatography was used to identify the content of Radix Aconiti Preparata, Radix Notoginseng and Radix Angelicae Sinensis, and second derivative spectrometry was used for the determination of aconitine in TQP. RESULTS: The positions of the spots of the three experimental samples were the same as those of the control sample, respectively. The calibration curve for aconitine was linear within the range of 0.04-0.26 g/L (r= 0.9994), the average recovery rate of aconitine was 99.4% and the relative standard deviation (RSD) was 1.20% . CONCLUSION: The method employed in this study is simple, accurate and can be used in quality control of TQP. |
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| Keywords: | Tongluo Quebi Pill Radix Aconiti Preparata Radix Notoginseng Radix Angelicae Sinensis aconitine thin layer chromatography second derivative spectrometry |
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