| 诺丽果肉化学成分研究 |
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| 引用本文： | 何其伟,吴培云,梁益敏,项晨,杜子伟,王刚. 诺丽果肉化学成分研究[J]. 中成药, 2012, 34(9): 1729-1733 |
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| 作者姓名： | 何其伟 吴培云 梁益敏 项晨 杜子伟 王刚 |
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| 作者单位： | 安徽中医学院药学院现代中药安徽省重点实验室 |
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| 摘 要： | 目的研究诺丽果肉的化学成分。方法利用硅胶、RP-18、Sephadex LH-20等柱色谱手段进行分离,根据理化性质和波谱分析鉴定化合物的结构。结果从乙醇提取物的乙酸乙酯部分和正丁醇部分中分离得到12个化合物,分别鉴定为β-谷甾醇(1)、乌苏酸(2)、莨菪亭(3)、邻苯二甲酸二甲酯(4)、4-epi-dunnisinin(5)、(24S)-ergost-7-en-3β-ol(6)、19-羟基-乌苏酸(7)、胡萝卜苷(8)、丁二酸(9)、1-O-(3’-methylbut-3’-enyl)-β-D-glucopyranose(10)、borreriagenin(11)、3-methylbut-3-enyl-6-O-β-D-glucopyranosyl-β-D-glucopyranoside(12)。结论化合物4为首次从该属植物中分离得到。
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| 关 键 词： | 诺丽 果肉 化学成分 结构鉴定 |
Chemical constituents of the sarcocarp of Morinda citrifolia |
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| HE Qi-wei,WU Pei-yun,LIANG Yi-min,XIANG Chen,DU Zi-wei,WANG Gang. Chemical constituents of the sarcocarp of Morinda citrifolia[J]. Chinese Traditional Patent Medicine, 2012, 34(9): 1729-1733 |
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| Authors: | HE Qi-wei WU Pei-yun LIANG Yi-min XIANG Chen DU Zi-wei WANG Gang |
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| Affiliation: | (Department of Pharmacology,Anhui College of Traditional Chinese Medicine & Anhui Key Laboratory of Modernized Chinese Medicine,Hefei 230031,China) |
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| Abstract: | AIM To study the chemical constituents in the fruit of Morinda citrifolia.METHODS The compounds were separated by repeated silica gel,RP-18 and Sephadex LH-20 chromatographies.Their structures were elucidated on the basis of chemical evidence and spectral data.RESULTS Twelve compounds were isolated and identified as β-sitosterol(1),ursolic acid(2),scopoletin(3),dimethyl phthalate(4),4-epi-dunnisinin(5),(24S)-ergost-7-en-3β-ol(6),19-hydroxyl-ursolic acid(7),daucosterol(8),succinic acid(9),1-O-(3′-methylbut-3′-enyl)-β-D-glucopyranose(10),borreriagenin(11),3-methylbut-3-enyl-6-O-β-D-glucopyranosyl-β-D-glucopyranoside(12).CONCLUSION Compound 4 was isolated from Morinda L.for the first time. |
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| Keywords: | Morinda citrifolia sarcocarp component structure identification |
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