| RP-HPLC测定好娃友口服液中橙皮苷的含量 |
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| 引用本文： | 张琦,赵因,艾春梅. RP-HPLC测定好娃友口服液中橙皮苷的含量[J]. 华西药学杂志, 2001, 16(1): 52-53 |
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| 作者姓名： | 张琦 赵因 艾春梅 |
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| 作者单位： | 四川恩威中医药研究所, |
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| 摘 要： | 目的 :建立好娃友口服液中橙皮苷的含量测定方法。方法 :采用甲醇溶解稀释样品 ,Shim packCLC ODS柱 ( 5 μm ,15 0mm× 6 0mm) ,以甲醇 水 ( 38∶6 2 )为流动相 ,检测波长 2 85nm。 结果 :橙皮苷进样量在 0 18～ 1 45 μg范围内线性关系良好 (r=0 9999) ,平均加样回收率为 10 0 1% (n =5 ,RSD =1 84% )。结论 :该法可用于好娃友口服液的质量控制
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| 关 键 词： | 高效液相色谱法 橙皮苷 好娃友口服液 |
| 文章编号： | 1006-0103(2001)01-0052-02 |
| 修稿时间： | 2000-08-01 |
DETERMINATION OF HESPERIDIN IN HAOWAYOU ORAL SOLUTION BY RP-HPLC |
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| ZHANG Qi,ZHAO Yin,AI Chun-mei. DETERMINATION OF HESPERIDIN IN HAOWAYOU ORAL SOLUTION BY RP-HPLC[J]. West China Journal of Pharmaceutical Sciences, 2001, 16(1): 52-53 |
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| Authors: | ZHANG Qi ZHAO Yin AI Chun-mei |
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| Abstract: | OBJECTIVE:To establish an HPLC method for determination of hesperidin in Haowayou oral solution.METHODS:The content of hesperidin in Haowayouoral solution was determined by RP-HPLC.The condition was ODS column,（5 μm ，150 mm ×6.0 mm）; methanol-water=38∶62 as mobile phase, and detective wavelength was 285 nm.RESULTS:Within the range of 0.18～1.45 μg, hesperidin presented a fine linear relationship between amount and peak area(r=0.9999).The average recovery in sample was 100.1%(n=5,RSD=1.84%). CONCLUSION:The established HPLC method could be used for determination of hesperidin in Haowayou oral solution. |
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| Keywords: | HPLC Hesperidin Haowayou oral solution |
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