| 八宝眼粉质量标准的研究 |
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| 引用本文： | 干国平,杨艳芳,肖佐强. 八宝眼粉质量标准的研究[J]. 中国医院药学杂志, 2004, 24(4): 210-211 |
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| 作者姓名： | 干国平 杨艳芳 肖佐强 |
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| 作者单位： | 1. 湖北中医学院,湖北,武汉,430061
2. 武汉市中药饮片厂,湖北,武汉,430022 |
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| 摘 要： | 目的:建立八宝眼粉的质量控制方法.方法:采用化学反应和薄层色谱法(TLC)鉴别方中炉甘石、人工牛黄、冰片;采用气相色谱法(GC)测定冰片的含量.结果:鉴别效果满意;冰片在0.09808～0.78464 μg范围内呈良好的线性关系,平均加样回收率为101.5%,RSD=1.40%(n=5).结论:本方法简便、快速准确,可作为该制剂质量控制方法.
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| 关 键 词： | 八宝眼粉 气相色谱法 冰片 含量测定 |
| 文章编号： | 1001-5213(2004)04-0210-02 |
| 修稿时间： | 2003-06-04 |
Study on the quality standard for Babao eye-powder |
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| GAN Guo Ping,YANG Yan Fang,XIAO Zhuo Qiang. Study on the quality standard for Babao eye-powder[J]. Chinese Journal of Hospital Pharmacy, 2004, 24(4): 210-211 |
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| Authors: | GAN Guo Ping YANG Yan Fang XIAO Zhuo Qiang |
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| Abstract: | OBJECTIVE To establish a quality standard for Babao Eye Powder. METHODS Galamina?Artificial calculus bovis and synthetic borneol were indentity by chemical reaction and TLC; synthetic Borneol was determined by GC. RESULTS The average recovery was 101.5% ,RSD= 1.40% ( n =5).CONCLUSIONS The methods are suitable for the quality control of the powder. |
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| Keywords: | Babao eye powder GC synthetic borneol assay |
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